REACTIONS OF DICHLOROMETHANE WITH THIOANIONS .1. PREPARATION OF BIS(N,N-DIALKYLTHIOCARBAMOYLTHIO)METHANES

被引：4

作者：

CESPEDES, C

VEGA, JC

机构：

[1] Facultad de Química, Pontificia Universidad Católica de Chile, Correo 22, Santiago

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 1994年 / 90卷 / 1-4期

关键词：

THIOANIONS; DICHLOROMETHANE; PHASE TRANSFER CATALYST; IR SPECTRA;

D O I：

10.1080/10426509408016397

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The preparation of some bis(N,N-dialkylthiocarbamoylthio)methanes, mainly published in the patent literature, is described. The method is based on the reaction of sodium N,N-dialkyldithiocarbamates in water with dichloromethane catalyzed by poly(ethylene glycol) 1,500. The yields are 50-80%.

引用

页码：155 / 158

页数：4

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