AN APPARATUS FOR THE EFFICIENT REMOVAL OF H2O FROM REACTION MIXTURES

被引：6

作者：

BARTA, NS ^{[1
]}

PAULVANNAN, K ^{[1
]}

SCHWARZ, JB ^{[1
]}

STILLE, JR ^{[1
]}

机构：

[1] MICHIGAN STATE UNIV,DEPT CHEM,E LANSING,MI 48824

来源：

SYNTHETIC COMMUNICATIONS | 1994年 / 24卷 / 04期

基金：

美国国家科学基金会;

关键词：

D O I：

10.1080/00397919408011509

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

An apparatus has been designed that facilitates the azeotropic removal of H2O from a reaction mixture. Representative condensation reactions in which this apparatus was used include acetal, imine, and enamine formation.

引用

页码：583 / 590

页数：8

共 21 条

[1] STUDIES OF THE REGIOSPECIFIC 3-AZA-COPE REARRANGEMENT PROMOTED BY ELECTROPHILIC REAGENTS [J].

BARTA, NS ;

COOK, GR ;

LANDIS, MS ;

STILLE, JR .

JOURNAL OF ORGANIC CHEMISTRY, 1992, 57 (26) :7188-7194

[2] THE PREPARATION OF METHYL ESTERS [J].

CLINTON, RO ;

LASKOWSKI, SC .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1948, 70 (09) :3135-3136

[3] A convenient method for the determination of water in petroleum and other organic emulsions [J].

Dean, EW ;

Stark, DD .

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY-US, 1920, 12 :486-490

[4]

HARRISON HR, 1968, CHEM IND-LONDON, P1568

[5] CHEMISTRY OF CARBANIONS .19. ALKYLATION OF ENOLATES FROM UNSYMMETRICAL KETONES [J].

HOUSE, HO ;

GALL, M ;

OLMSTEAD, HD .

JOURNAL OF ORGANIC CHEMISTRY, 1971, 36 (16) :2361-&

[6] STUDIES ON ENAMINOKETONES [J].

JIRKOVSKY, I .

CANADIAN JOURNAL OF CHEMISTRY, 1974, 52 (01) :55-65

[7]

JORDAAN JH, 1963, J ORG CHEM, V28, P1395

[8]

Lucke E., 1961, ORG SYNTH, V41, p[65, 808]

[9] Concerning simple enamines with tertiary bounded nitrogen [J].

Mannich, C ;

Davidsen, H .

BERICHTE DER DEUTSCHEN CHEMISCHEN GESELLSCHAFT, 1936, 69 :2106-2112

[10]

NATELSON S, 1955, ORG SYNTH C, V3, P381

← 1 2 3 →