Crystal structure of hexaaquanickel(II) bis{5-bromo-7-[(2-hydroxyethyl)amino]-1-methyl-6-oxidoquinolin-1-ium-3-sulfonate} monohydrate

被引：0
作者：
Hai Le Thi Hong [1 ]
Vinh Nguyen Thi Ngoc [1 ]
Anh Do Thi Van [1 ]
Van Meervelt, Luc [2 ]
机构：
[1] Hanoi Natl Univ Educ, Chem Dept, 136 Xuan Thuy, Hanoi, Vietnam
[2] KU Leuven Univ Leuven, Dept Chem, Celestijnenlaan 200F Bus 2404, B-3001 Heverlee, Belgium
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2016年 / 72卷
关键词：
crystal structure; quinoline; hydrogen bonding; pi-pi stacking;
D O I：
10.1107/S2056989016012408
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The asymmetric unit of the title compound, [Ni(H2O)(6)](C12H12BrN2O5S)(2)center dot H2O, contains a half hexaaquanickel(II) complex cation with the Ni-II ion lying on an inversion center, one 5-bromo-7-[(2-hydroxyethyl) amino]-1-methyl-6-oxidoquinolin-1-ium-3-sulfonate (QAO) anion and a half lattice water molecule on a twofold rotation axis. In the crystal, QAO anions are stacked in a column along the c axis by pi-pi stacking interactions [centroid-centroid distances 3.5922 (10)-3.7223 (11) angstrom]. The columns are interlinked by hexaaquanickel(II) cations through O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds.
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收藏
页码：1242 / +
页数：10
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