THE SYNTHESIS AND CHARACTERIZATION OF DECAPHENYLTITANOCENE DICHLORIDE, [TI(ETA-5-C5PH5)2CL2], AND OF [TI(ETA-5-C5PH5)((C6H11)7SI7O12)], THE 1ST PENTAPHENYLCYCLOPENTADIENYL POLYHEDRAL OLIGOSILSESQUIOXANE

被引：28

作者：

FIELD, LD

LINDALL, CM

MASCHMEYER, T

MASTERS, AF

机构：

来源：

AUSTRALIAN JOURNAL OF CHEMISTRY | 1994年 / 47卷 / 06期

关键词：

D O I：

10.1071/CH9941127

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The syntheses and characterization of the compounds [Ti(eta5-C5Ph5)2Cl2] and [Ti(eta5-C5Ph5)((C-C6H11)7Si7O12)] by infrared, H-1, C-13 and Si-29 n.m.r. and mass spectroscopy are described.

引用

页码：1127 / 1132

页数：6

共 23 条

[1] THE CRYSTAL AND MOLECULAR-STRUCTURE OF (MU(5)-PENTAPHENYLCYCLOPENTADIENYL) (MU(5)-CYCLOPENTADIENYL)IRON(II), 1,2,3,4,5-PENTAPHENYLFERROCENE, [FE(C5PH5)(C5H5)] [J].

ARONEY, MJ ;

BUYS, IE ;

DENNIS, GD ;

FIELD, LD ;

HAMBLEY, TW ;

LAY, PA ;

MASTERS, AF .

POLYHEDRON, 1993, 12 (16) :2051-2056

[2] (ETA-5-PENTAPHENYLCYCLOPENTADIENYL)(1-(ETA-6-PHENYL)-2,3,4,5-TETRAPHENYLCYCLOPENTADIENYL) IRON(II), [FE(ETA-5-C5PH5)((ETA-6-C6H5)C5PH4)], A LINKAGE ISOMER OF DECAPHENYLFERROCENE [J].

BROWN, KN ;

FIELD, LD ;

LAY, PA ;

LINDALL, CM ;

MASTERS, AF .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1990, (05) :408-410

[3] MODELS OF SURFACE-CONFINED METALLOCENE DERIVATIVES [J].

BUYS, IE ;

HAMBLEY, TW ;

HOULTON, DJ ;

MASCHMEYER, T ;

MASTERS, AF ;

SMITH, AK .

JOURNAL OF MOLECULAR CATALYSIS, 1994, 86 (1-3) :309-318

[4] SYNTHESIS AND MOLECULAR-STRUCTURE OF CHLOROBIS(TETRAPHENYLCYCLOPENTADIENYL)TITANIUM(III) - SYNTHESIS AND VARIABLE-TEMPERATURE H-1-NMR STUDY OF DICHLOROBIS(TETRAPHENYLCYCLOPENTADIENYL)TITANIUM(IV) [J].

CASTELLANI, MP ;

GEIB, SJ ;

RHEINGOLD, AL ;

TROGLER, WC .

ORGANOMETALLICS, 1987, 6 (12) :2524-2531

[5] ELECTROSYNTHESIS OF ALKYL AND ARYLOXY TITANIUM(III) COMPLEXES - ELECTROCHEMICAL AND SPECTROSCOPIC CHARACTERIZATION [J].

CHALOYARD, A ;

DORMOND, A ;

TIROUFLET, J ;

MURR, NE .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1980, (05) :214-216

[6]

ELMURR N, 1980, J CHEM SOC CHEM COMM, P446

[7] OLEFIN POLYMERIZATION BY VANADIUM-CONTAINING POLYHEDRAL OLIGOMETALLASILSESQUIOXANES [J].

FEHER, FJ ;

WALZER, JF ;

BLANSKI, RL .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1991, 113 (09) :3618-3619

[8] SYNTHESIS AND CHARACTERIZATION OF VANADIUM-CONTAINING SILSESQUIOXANES [J].

FEHER, FJ ;

WALZER, JF .

INORGANIC CHEMISTRY, 1991, 30 (08) :1689-1694

[9] SILSESQUIOXANES AS MODELS FOR SILICA SURFACES [J].

FEHER, FJ ;

NEWMAN, DA ;

WALZER, JF .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (05) :1741-1748

[10] REACTIONS OF INCOMPLETELY-CONDENSED SILSESQUIOXANES WITH PENTAMETHYLANTIMONY - A NEW SYNTHESIS OF METALLASILSESQUIOXANES WITH IMPORTANT IMPLICATIONS FOR THE CHEMISTRY OF SILICA SURFACES [J].

FEHER, FJ ;

BUDZICHOWSKI, TA ;

RAHIMIAN, K ;

ZILLER, JW .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (10) :3859-3866

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