Immobilization Effect of Morphological, Thermal and Optical Properties in Biotemplate on Zinc Oxide Nanocomposite from Chitosan

被引:3
作者
Karpuraranjith, M. [1 ]
Thambidurai, S. [1 ]
机构
[1] Alagappa Univ, Sch Chem Sci, Dept Ind Chem, Bionanomat Res Lab, Karaikkudi 630003, Tamil Nadu, India
关键词
Biotemplate; zinc oxide; nanocomposite; immobilization effect; chitosan matrix; chemical precipitation; microcrystalline; high surface area; thermal stability; nanotechnology;
D O I
10.1142/S0219581X17600456
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Biotemplate-based zinc oxide nanocomposite was effectively prepared via simple chemical precipitation route. The functional groups of amino (-NH2), hydroxyl (-OH) and O-Zn-O were confirmed and characterized by FTIR spectroscopy. The structural and morphological properties were confirmed by XRD, UV-Vis DRS, HR-SEM and TEM analyses. The elemental composition of carbon, nitrogen, zinc and oxygen was confirmed by energy-dispersive X-ray analysis (EDAX) and Brunauer-Emmett-Teller high surface area of materials was estimated to be 52.49 m(2)/g, respectively. Thermogravimetric analysis (TGA) shows that biotemplate on zinc oxide nanocomposite has higher thermal stability than chitosan matrix. The results demonstrate that biotemplate on zinc oxide matrix causes immobilization effect among the two components. Therefore, chitosan-ZnO nanocomposite has a microcrystalline morphological structure and also good thermal stability, so it can be a promising material for sensors, medical, tissue engineering and wastewater treatment applications.
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页数:7
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