ANALYSIS OF SODIUM POLYCARBOXYLATES IN DETERGENTS BY SIZE EXCLUSION CHROMATOGRAPHY

被引：7

作者：

KRUSCHE, G

ILLERT, J

MANDERY, H

机构：

[1] BASF AG,ZSZ ANALYT DEPT,W-6700 LUDWIGSHAFEN,GERMANY

[2] BENCKISER PROD GMBH,QUAL CONTROL M TQ,W-6700 LUDWIGSHAFEN,GERMANY

来源：

CHROMATOGRAPHIA | 1991年 / 31卷 / 1-2期

关键词：

SIZE EXCLUSION CHROMATOGRAPHY; POLYCARBOXYLATES IN DETERGENTS; PREPARATIVE GPC;

D O I：

10.1007/BF02290490

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

This paper describes the quantitative analysis and preparative isolation of sodium polycarboxylates in detergents by means of gel permeation chromatography. An analytical monitoring method separates the polymers from other low molecular detergent ingredients within 10 minutes. There is no separation of the various molecular weight polycarboxylate macromolecules themselves. They elute from the column as a single narrow peak at the exclusion volume. A second preparative gel filtration method allows isolation of polycarboxylates in amounts necessary for further characterization. Appropriate sample pretreatments and possible interferences are discussed.

引用

页码：17 / 20

页数：4