SYNTHESIS AND CHARACTERIZATION OF A PYRIDINE ADDUCT OF BIS(IRONTETRACARBONYL)GERMANIUM(IV)

被引:8
|
作者
LEI, D [1 ]
HAMPDENSMITH, MJ [1 ]
DUESLER, EN [1 ]
机构
[1] UNIV NEW MEXICO,CTR MICROENGINEERED CERAM,ALBUQUERQUE,NM 87131
基金
美国国家科学基金会;
关键词
D O I
10.1016/S0277-5387(00)81306-6
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The reaction of [(CO)4FeGeBr2]2 (1) with Na2Fe(CO)4 (2) in the presence of pyridine results in the formation of [{(CO)4Fe}2Ge·2py] (3) in high yield. A single crystal X-ray diffraction study of 3 reveals that the local environment around germanium is severely distorted from tetrahedral coordination. © 1990.
引用
收藏
页码:1127 / 1129
页数:3
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