EXTRACTION OF VANADIUM FROM PETROLEUM COKE SAMPLES BY MEANS OF MICROWAVE WET ACID DIGESTION

被引:14
作者
ALVARADO, J [1 ]
ALVAREZ, M [1 ]
CRISTIANO, AR [1 ]
MARCO, LM [1 ]
机构
[1] UNIV NACL PEDRO ENRIQUE URENA,DEPT FIS,SANTO DOMINGO,DOMINICAN REP
关键词
coke; petroleum products; vanadium;
D O I
10.1016/0016-2361(90)90271-Q
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
Certified coal standards and Venezuelan petroleum coke samples were submitted to microwave acid digestion to evaluate the convenience of this procedure for the extraction of their vanadium content. The solution and the solid residue remaining after microwave treatment were separated by filtration and each one was analysed for vanadium. The solutions were analysed by graphite furnace atomic absorption spectrometry (GFAAS), the solid residues and the untreated samples of petroleum coke were analysed by X-ray fluorescence spectrometry. The results of the analyses showed total extraction of the vanadium after a microwave heating period of approximately 15 min per sample. © 1990.
引用
收藏
页码:128 / 130
页数:3
相关论文
共 17 条
[1]   WET ASHING OF SOME BIOLOGICAL SAMPLES IN A MICROWAVE OVEN [J].
ABUSAMRA, A ;
MORRIS, JS ;
KOIRTYOHANN, SR .
ANALYTICAL CHEMISTRY, 1975, 47 (08) :1475-1477
[2]   COMPARISON OF CONVENTIONAL AND MICROWAVE WET ACID DIGESTION PROCEDURES FOR THE DETERMINATION OF IRON, NICKEL AND VANADIUM IN COAL BY ELECTROTHERMAL ATOMIZATION ATOMIC-ABSORPTION SPECTROMETRY [J].
ALVARADO, J ;
LEON, LE ;
LOPEZ, F ;
LIMA, C .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1988, 3 (01) :135-138
[3]  
BLUST R, 1985, ATOM SPECTROSC, V6, P163
[4]   FLOW-INJECTION AND MICROWAVE-OVEN SAMPLE DECOMPOSITION FOR DETERMINATION OF COPPER, ZINC AND IRON IN WHOLE-BLOOD BY ATOMIC-ABSORPTION SPECTROMETRY [J].
BURGUERA, M ;
BURGUERA, JL ;
ALARCON, OM .
ANALYTICA CHIMICA ACTA, 1986, 179 :351-357
[5]   CLOSED-VESSEL MICROWAVE DISSOLUTION AND COMPREHENSIVE ANALYSIS OF STEEL BY DIRECT-CURRENT PLASMA ATOMIC EMISSION-SPECTROMETRY [J].
FERNANDO, LA ;
HEAVNER, WD ;
GABRIELLI, CC .
ANALYTICAL CHEMISTRY, 1986, 58 (02) :511-512
[6]  
GIAUQUE RD, 1983, ANAL CHEM, V45, P671
[7]   LARGE BATCH SEALED TUBE DECOMPOSITION OF GEOCHEMICAL SAMPLES BY MEANS OF A LAYERED HEATING BLOCK [J].
HALE, M ;
THOMPSON, M ;
LOVELL, J .
ANALYST, 1985, 110 (03) :225-228
[8]   MICROWAVE-ENERGY FOR ACID DECOMPOSITION AT ELEVATED-TEMPERATURES AND PRESSURES USING BIOLOGICAL AND BOTANICAL SAMPLES [J].
KINGSTON, HM ;
JASSIE, LB .
ANALYTICAL CHEMISTRY, 1986, 58 (12) :2534-2541
[9]  
LAMOTHE PJ, 1986, J ANAL CHEM, V58, P1811
[10]   MICROWAVE DIGESTION TECHNIQUES IN THE SEQUENTIAL EXTRACTION OF CALCIUM, IRON, CHROMIUM, MANGANESE, LEAD, AND ZINC IN SEDIMENTS [J].
MAHAN, KI ;
FODERARO, TA ;
GARZA, TL ;
MARTINEZ, RM ;
MARONEY, GA ;
TRIVISONNO, MR ;
WILLGING, EM .
ANALYTICAL CHEMISTRY, 1987, 59 (07) :938-945