DETERMINATION OF BROMINE IN ORGANIC-COMPOUNDS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：5
作者：
JAIN, A [1 ]
VERMA, A [1 ]
VERMA, KK [1 ]
机构：
[1] RANI DURGAVATI UNIV,DEPT CHEM,JABALPUR 482001,MADHYA PRADESH,INDIA
来源：
TALANTA | 1990年 / 37卷 / 06期
关键词：
D O I：
10.1016/0039-9140(90)80202-Q
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A method is proposed for the determination of bromine in organic compounds (which may also contain chlorine and iodine) by oxygen-flask combustion of the compound followed by pre-column reaction of bromide with acetanilide and 2-iodosobenzoic acid to form 4-bromoacetanilide which is then chromatographed on an ODS column with a mobile phase of methanol: water, 65:35 v/v, detection at 240 nm, and 4-N-acetylaminotoluene as internal standard. The method is rapid and precise (RSD ≤ 1%), and applicable to a variety of bromine-containing organic compounds; the limit of detection is 0.2 ng of bromine. © 1990.
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页码：595 / 598
页数：4
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