SIMULTANEOUS DETERMINATION OF TRACE-METALS IN HUMAN HAIR BY DYNAMIC ION-EXCHANGE CHROMATOGRAPHY

被引:23
作者
STURARO, A
PARVOLI, G
DORETTI, L
ZANCHETTA, S
ALLEGRI, G
BATTISTON, G
机构
[1] UNIV PADUA,DIPARTIMENTO SCI FARMACEUT,I-35100 PADUA,ITALY
[2] CNR,CORSO STATI UNITI 4,IST CHIM & TECNOL RADIOELEMENTI,I-35020 PADUA,ITALY
关键词
ION EXCHANGE; LIQUID CHROMATOGRAPHY; HAIR; TRACE METALS;
D O I
10.1016/0003-2670(93)80616-S
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The simultaneous determination of six metal ions (Cu2+, Zn2+, Ni2+, Mn2+, Co2+, Pb2+) by using dynamic ion-exchange chromatography is proposed. The method was applied to the analysis of human hair after HNO3-HClO4 digestion, with detection limits of ca. 1 mug g-1 for all the metals examined, using Co as an internal standard. The quantitative data were confirmed by analysing the same hair samples by atomic absorption spectrometry and x-ray fluorescence spectrometry.
引用
收藏
页码:163 / 170
页数:8
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