SELECTIVE H-2, H-2 1D-TOCSY NMR-SPECTROSCOPY FOR SIGNAL ASSIGNMENT IN PERDEUTERATED COMPOUNDS

被引：5

作者：

MONS, HE ^{[1
]}

BERGANDER, K ^{[1
]}

GUNTHER, H ^{[1
]}

机构：

[1] UNIV SIEGEN,FACHBEREICH 8,OC 2,W-5900 SIEGEN,GERMANY

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1993年 / 31卷 / 05期

关键词：

NMR; H-2; 1D-TOCSY; H-2-TOCSY; MAGNETIZATION TRANSFER; SELECTIVE EXCITATION; PYRIDINE-D(S); DEUTERIATED CYCLOHEXANES;

D O I：

10.1002/mrc.1260310517

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The ID-TOCSY experiment for H-2 NMR is introduced and applications for signal assignments are illustrated with the spectra of pyridine-d5 and iodo- and chlorocyclohexane-d11. The potential of the method for the analysis of overlapping H-2 spectra is demonstrated.

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页码：509 / 511

页数：3

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