Ultralong Coordination Polymers Microtubes: Facile Microwave Preparation and Characterization

被引：3

作者：

Ji, Yanhua ^{[1
]}

Yan, Haiming ^{[1
]}

Wang, Lei ^{[1
]}

Luo, Yuwen ^{[1
]}

Guo, Dongdong ^{[1
]}

Bai, Linjie ^{[1
]}

Zhong, Shengliang ^{[1
]}

机构：

[1] Jiangxi Normal Univ, Coll Chem & Chem Engn, 99 Ziyang Rd, Nanchang 330022, Jiangxi, Peoples R China

来源：

CURRENT MICROWAVE CHEMISTRY | 2014年 / 1卷 / 01期

关键词：

Coordination polymers; drug delivery; microstructure; microtubes; microwave; MOFs; nickel; nanoscale; ultralong; soft materials;

D O I：

10.2174/2213335601666131223234744

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A facile microwave heating method was applied to the preparation of nickel-dimethylglyoxime microtubes in half an hour, using nickel nitrate and diacetyldioxime as starting reagents, in the absence of template or surfactant. The products were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM) and infrared spectroscopy (IR). Results show that those microtubes with lengths of 100-500 mu m and diameters of 10-15 mu m are hollowed. Furthermore, these microtube are hollowed via an inside to outside process under microwave irradiation. For comparison, experiments were carried out under refluxing conditions.

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页码：2 / 5

页数：4

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