DETERMINATION OF TRACE LEVELS OF METAL-IONS IN WATER SAMPLES BY INDUCTIVELY-COUPLED PLASMA-MASS SPECTROMETRY AFTER ONLINE PRECONCENTRATION ON SO3-OXINE CM-CELLULOSE

被引：30
作者：
HUANG, KS [1 ]
JIANG, SJ [1 ]
机构：
[1] NATL SUN YAT SEN UNIV,DEPT CHEM,KAOHSIUNG 804,TAIWAN
来源：
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1993年 / 347卷 / 6-7期
关键词：
D O I：
10.1007/BF00323965
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A method utilizing a miniature chelated ion-exchanger column of SO3-oxine CM-cellulose has been developed to increase the sensitivity for multielement measurements by inductively coupled plasma mass spectrometry (ICP-MS). This matrix/analyte separation and preconcentration technique has been used to preconcentrate Mn, Co, Ni, Cu, Cd, and Pb from natural water samples. The multielement detection limits are in the low ppt (pg/mL) range. This FIA-ICP-MS method has been applied to the determination of various trace levels of metal ions in riverine reference material SLRS-2 and open ocean seawater reference material NASS-3.
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页码：238 / 242
页数：5
相关论文
共 24 条
[1]   DETERMINATION OF TRACE-METALS IN AN OPEN OCEAN WATER REFERENCE MATERIAL BY INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].
BEAUCHEMIN, D ;
MCLAREN, JW ;
MYKYTIUK, AP ;
BERMAN, SS .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1988, 3 (02) :305-308
[2]   DETERMINATION OF TRACE-METALS IN REFERENCE WATER STANDARDS BY INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY WITH ONLINE PRECONCENTRATION [J].
BEAUCHEMIN, D ;
BERMAN, SS .
ANALYTICAL CHEMISTRY, 1989, 61 (17) :1857-1862
[3]   DETERMINATION OF TRACE-METALS IN A RIVER WATER REFERENCE MATERIAL BY INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].
BEAUCHEMIN, D ;
MCLAREN, JW ;
MYKYTIUK, AP ;
BERMAN, SS .
ANALYTICAL CHEMISTRY, 1987, 59 (05) :778-783
[4]   INDUCTIVELY COUPLED PLASMA MASS - SPECTROMETRY IN HYPHENATION - A MULTIELEMENTAL ANALYSIS TECHNIQUE WITH ALMOST UNLIMITED POTENTIAL [J].
BEAUCHEMIN, D .
TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 1991, 10 (02) :71-R7
[5]   DETERMINATION OF URANIUM IN ENVIRONMENTAL-SAMPLES USING INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY [J].
BOOMER, DW ;
POWELL, MJ .
ANALYTICAL CHEMISTRY, 1987, 59 (23) :2810-2813
[6]   DETERMINATION OF TRACE-ELEMENTS IN GEOLOGICAL SAMPLES BY INDUCTIVELY COUPLED PLASMA SOURCE-MASS SPECTROMETRY [J].
DATE, AR ;
GRAY, AL .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1985, 40 :115-122
[7]  
GRAY AL, 1987, J ANAL ATOM SPECTROM, V2, P595
[8]   INFLUENCE OF INSTRUMENT PARAMETERS ON NONSPECTROSCOPIC INTERFERENCES IN INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY [J].
GREGOIRE, DC .
APPLIED SPECTROSCOPY, 1987, 41 (05) :897-903
[9]   MINIMIZATION OF INTERFERENCES IN INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY USING ONLINE PRECONCENTRATION [J].
HEITHMAR, EM ;
HINNERS, TA ;
ROWAN, JT ;
RIVIELLO, JM .
ANALYTICAL CHEMISTRY, 1990, 62 (08) :857-864
[10]   DEVELOPMENTS IN PLASMA SOURCE-MASS SPECTROMETRY [J].
HIEFTJE, GM ;
VICKERS, GH .
ANALYTICA CHIMICA ACTA, 1989, 216 (1-2) :1-24
123