CRYSTAL-STRUCTURE OF PARAPHENOLAMMONIUM DIHYDROGEN PHOSPHATE

被引：9
作者：
SOUMHI, EH
DRISS, A
JOUINI, T
机构：
[1] Département de chimie, Faculté des Sciences de Tunis, 1060 Tunis, Campus universitaire
来源：
MATERIALS RESEARCH BULLETIN | 1994年 / 29卷 / 07期
关键词：
ORGANIC PHOSPHATES; ORTHOPHOSPHATES;
D O I：
10.1016/0025-5408(94)90202-X
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
(1-4,HOC6H4NH3)H2PO4, Mr=206.98, Orthorhombic, P2(1)2(1)2(1), a=6.155(2), b=7.514(3), c=18.704(7)angstrom, V=865.9(1)angstrom3,Z=4, D(m)=1.57, D(x)=1.59gcm-3, mu=3.157cm-1, T=298K, R=0.037 (wR=0.027) for 868 independent reflections. The structure was determined by single crystal X-Ray diffraction.It consists of an alternate stacking of (H2PO4)- tetrahedra sheets and (HOC6H4NH3)+ cation sheets. The (H2PO4)-groups are associated to form infinite chains (H2PO4), with internal P-P distances of 4.554(1)angstrom, and are connected to the organic planes thanks to strong hydrogen bonds.
引用
收藏
页码：767 / 775
页数：9
相关论文
共 13 条
[1]   STRUCTURE OF ETHANOLAMMONIUM CYCLO-TETRAPHOSPHATE [J].
AVERBUCHPOUCHOT, MT ;
DURIF, A ;
GUITEL, JC .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1988, 44 :1416-1418
[2]   STRUCTURE OF DISODIUM ETHYLENEDIAMMONIUM BIS[MONOHYDROGENTETRAOXOPHOSPHATE(V)] HEXAHYDRATE [J].
AVERBUCHPOUCHOT, MT ;
DURIF, A ;
GUITEL, JC .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1987, 43 :1896-1898
[3]  
AVERBUCHPOUCHOT MT, 1992, EUR J SOL STATE INOR, V29, P411
[4]   STRUCTURES OF ETHYLENEDIAMMONIUM MONOHYDROGENTETRAOXOPHOSPHATE(V) AND ETHYLENEDIAMMONIUM MONOHYDROGENTETRAOXOARSENATE(V) [J].
AVERBUCHPOUCHOT, MT ;
DURIF, A .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1987, 43 :1894-1896
[5]  
BUSING WR, 1979, ORXFLS4 CRISTALLOGRA
[6]  
ISABEV Z, 1982, RUSS J INORG CHEM, V26, P1086
[7]  
KAMMOUN S, 1990, J SOLID STATE CHEM, V89, P67
[8]   CRYSTAL STRUCTURE OF 2-AMINO-ETHANOL PHOSPHATE [J].
KRAUT, J .
ACTA CRYSTALLOGRAPHICA, 1961, 14 (11) :1146-&
[9]  
MAIN P, 1980, MULTAN SYSTEM COMPUT
[10]   STRUCTURE OF PYRIDINIUM DIHYDROGENPHOSPHATE PHOSPHORIC-ACID [J].
MASSE, R ;
TORDJMAN, I .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1990, 46 :606-609
12