A NEW, HIGHLY EFFICIENT SYNTHESIS OF CONJUGATED NITROCYCLOALKENES

被引:21
作者
BALLINI, R
PALESTINI, C
机构
[1] Dipartimento di Scienze Chimiche dell'Università, I-62032 Camerino
关键词
D O I
10.1016/S0040-4039(00)77291-1
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Sodium borohydride reduction of alpha-nitrocycloalkanones and successive dehydration of the obtained beta-nitroalkanols, by acetylation and dehydroacetylation with basic alumina/DMAP, in refluxing dichloromethane, affords, in one-pot procedure, conjugated nitrocycloalkenes.
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页码:5731 / 5734
页数:4
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