C-13 SOLID-STATE NMR SPIN-LATTICE RELAXATION-TIME MEASUREMENTS OF COALS

被引:2
作者
BARRIE, PJ [1 ]
MADRALI, ES [1 ]
KANDIYOTI, R [1 ]
机构
[1] UNIV LONDON IMPERIAL COLL SCI & TECHNOL,DEPT CHEM ENGN,LONDON SW7 2BY,ENGLAND
关键词
D O I
10.1021/ef00040a007
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
Spin-lattice (T1) relaxation times of C-13 nuclei have been measured on eight different coals in order to determine the best experimental conditions for recording C-13 single-pulse-excitation NMR spectra. It is found that a recycle delay of approximately 100 s is necessary to obtain quantitatively reliable spectra of coals using single-pulse-excitation methods.
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页码:479 / 481
页数:3
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