FLOW-INJECTION TITRATION - LINEAR OR LOGARITHMIC

被引:11
作者
CHEN, R [1 ]
RUZICKA, J [1 ]
CHRISTIAN, GD [1 ]
机构
[1] UNIV WASHINGTON,DEPT CHEM,CTR PROC ANALYT CHEM,BG-10,SEATTLE,WA 98195
关键词
D O I
10.1016/0039-9140(94)E0119-C
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A simple and rapid Continuous Flow Injection Titration method utilizing a pretitration step was developed to automate the assay of high sulfuric acid concentrations over a narrow range in an oil refinery stream. A Coulometric Flow Injection Titration method was developed to perform Karl Fisher titration. Multiple functions of the mixing chamber in these FIA titrations such as for pretitration dilution, and reduction of viscosity are discussed. The cell also serves as the detector. Appropriate combining of these functions allows FIA titrations to become a powerful tool in automating routine assays.
引用
收藏
页码:949 / 955
页数:7
相关论文
共 22 条
[2]  
BARROS FG, 1992, ANALYST, V117, P917
[3]   EXPLOITING STOPPED-FLOW INJECTION METHODS FOR QUANTITATIVE CHEMICAL-ASSAYS [J].
CHRISTIAN, GD ;
RUZICKA, J .
ANALYTICA CHIMICA ACTA, 1992, 261 (1-2) :11-21
[4]  
CHRISTIAN GD, 1991, ANAL CHEM, V63, P2407
[5]   FLOW-REVERSAL FLOW-INJECTION ANALYSIS - ENHANCEMENT OF FLOW-INJECTION TITRATIONS [J].
CLARK, GD ;
ZABLE, J ;
RUZICKA, J ;
CHRISTIAN, GD .
TALANTA, 1991, 38 (02) :119-124
[6]   APPLICATION OF FLOW-THROUGH TECHNIQUES TO DRUG DISSOLUTION STUDIES [J].
FEHER, Z ;
KOLBE, I ;
PUNGOR, E .
ANALYST, 1991, 116 (05) :483-487
[7]  
FURHMANN B, 1993, ANAL CHIM ACTA, V282, P397
[8]   FIA TITRATIONS OF SULFIDE, CYSTEINE AND THIOL-CONTAINING DRUGS WITH CHEMILUMINESCENT DETECTION [J].
GARCIA, IL ;
VINAS, P ;
GIL, JAM .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1993, 345 (11) :723-726
[9]   AUTOMATED FLOW-INJECTION SPECTROPHOTOMETRIC NON-AQUEOUS PSEUDOTITRATIONS OF AMINES AND THEIR HYDROHALIDE SALTS [J].
GEORGIOU, CA ;
KOUPPARIS, MA .
ANALYST, 1988, 113 (05) :755-760
[10]   FLOW-INJECTION ANALYSIS BY USING ACID-BASE OR METAL-LIGAND BUFFERS AND COLOR-INDICATORS [J].
ISHIBASHI, N ;
IMATO, T .
FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1986, 323 (03) :244-248