THE H-2,H-2-INADEQUATE EXPERIMENT - DETECTION OF ONE-SPIN AND 2-SPIN DOUBLE QUANTUM COHERENCES

被引：2

作者：

MONS, HE ^{[1
]}

BERGANDER, K ^{[1
]}

GUNTHER, H ^{[1
]}

机构：

[1] UNIV SIEGEN,FACHBEREICH 8,POSTFACH 101240,W-5900 SIEGEN,GERMANY

来源：

HELVETICA CHIMICA ACTA | 1993年 / 76卷 / 03期

关键词：

D O I：

10.1002/hlca.19930760308

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The INADEQUATE experiment for spin-1 nuclei has been extended to deuteron spin systems of the AX, AA'XX', and AA'MM'X type. Measurements with (3,3-D2)norcampher, 4-chloro(2,3,5,6-D4)pyridine, and (D5)pyridine revealed correlation peaks due to two-spin double quantum coherences and additional one-spin double quantum peaks with coordinates F1 = 2 omega(i) F2 = omega(i) (i = A, X) which were not observed in the Li-6,Li-6-INADEQUATE experiment described earlier.

引用

页码：1216 / 1218

页数：3

共 13 条

[1] BAX A, 1980, J AM CHEM SOC, V102, P2102
[2] ANALYSIS OF NETWORKS OF COUPLED SPINS BY MULTIPLE QUANTUM NMR
BRAUNSCHWEILER, L
BODENHAUSEN, G
ERNST, RR
[J]. MOLECULAR PHYSICS, 1983, 48 (03) : 535 - 560
[3] REACTIVITY OF 4-NITROPYRIDINE-N-OXIDE - PREPARATION OF 4-SUBSTITUTED DERIVATIVES OF PYRIDINE-N-OXIDE AND PYRIDINE
DENHERTOG, HJ
COMBE, WP
[J]. RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS-JOURNAL OF THE ROYAL NETHERLANDS CHEMICAL SOCIETY, 1951, 70 (07): : 581 - 590
[4] THE LI-6,LI-6-INADEQUATE EXPERIMENT - A NEW TOOL FOR 1D-NMR AND 2D-NMR STUDIES OF ORGANOLITHIUM COMPOUNDS
EPPERS, O
FOX, T
GUNTHER, H
[J]. HELVETICA CHIMICA ACTA, 1992, 75 (03) : 883 - 891
[5] VICINAL H-2/H-1 ISOTOPE SHIFTS FOR LI-6-NMR AND THE AGGREGATION BEHAVIOR OF PHENYLLITHIUM
EPPERS, O
GUNTHER, H
[J]. HELVETICA CHIMICA ACTA, 1992, 75 (08) : 2553 - 2562
[6] HOMONUCLEAR SCALAR LI-6,LI-6 SPIN-SPIN COUPLING - 1ST DIRECT OBSERVATION AND DETECTION VIA THE LI-6,LI-6 INADEQUATE EXPERIMENT
EPPERS, O
GUNTHER, H
KLEIN, KD
MAERCKER, A
[J]. MAGNETIC RESONANCE IN CHEMISTRY, 1991, 29 (10) : 1065 - 1067
[7] MODERN NMR-SPECTROSCOPY OF ORGANO-LITHIUM COMPOUNDS
GUNTHER, H
MOSKAU, D
BAST, P
SCHMALZ, D
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1987, 26 (12): : 1212 - 1220
[8] GUNTHER H, 1987, ANGEW CHEM, V99, P1242
[9] COMPLETE PROTON NUCLEAR MAGNETIC-RESONANCE ANALYSIS OF NORCAMPHOR
MARSHALL, JL
WALTER, SR
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1974, 96 (20) : 6358 - 6362
[10] RECENT JAPANESE WORK ON THE CHEMISTRY OF PYRIDINE 1-OXIDE AND RELATED COMPOUNDS
OCHIAI, E
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1953, 18 (05) : 534 - 551

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