Fabrication and Optical Characterization of Zinc Oxide Nanoparticles Prepared via a Simple Sol-gel Method

被引:59
作者
Hedayati, K. [1 ]
机构
[1] Arak Univ Technol, Dept Sci, Arak, Iran
关键词
Nanoparticle; Sol-gel; Zinc Oxide;
D O I
10.7508/jns.2015.04.010
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this research zinc oxide (ZnO) nano-crystalline powders were prepared by sol-gel method using zinc acetate. The ZnO nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), ultraviolet-visible (UV-Vis), Fourier transform infra-red (FT-IR) and energy dispersive X-ray (EDX) spectroscopy. The structure of nanoparticles was studied using XRD pattern. The crystallite size of ZnO nanoparticles was calculated by DebyeScherrer formula. Morphology of nano-crystals was observed and investigated using the SEM. The grain size of zinc oxide nanoparticles were in suitable agreement with the crystalline size calculated by XRD results. The optical properties of particles were studied with UV-Vis an FTIR absorption spectrum. The Raman spectrum measurements were carried out using a micro-laser Raman spectrometer forms the ZnO nanoparticles. At the end studied the effect of calcined temperature on the photoluminescence (PL) emission of ZnO nanoparticles. 2015 JNS All rights reserved
引用
收藏
页码:395 / 401
页数:7
相关论文
共 22 条
  • [1] Effect of pH on ZnO nanoparticle properties synthesized by sol-gel centrifugation
    Alias, S. S.
    Ismail, A. B.
    Mohamad, A. A.
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 499 (02) : 231 - 237
  • [2] STUDIES ON SEMICONDUCTING THIN-FILMS PREPARED BY THE SPRAY PYROLYSIS TECHNIQUE FOR PHOTOELECTROCHEMICAL SOLAR-CELL APPLICATIONS - PREPARATION AND PROPERTIES OF ZNO
    BAHADUR, L
    HAMDANI, M
    KOENIG, JF
    CHARTIER, P
    [J]. SOLAR ENERGY MATERIALS, 1986, 14 (02): : 107 - 120
  • [3] Effects of temperature on the ferromagnetism of Mn-doped ZnO nanoparticles and Mn-related Raman vibration
    Cong, CJ
    Liao, L
    Liu, QY
    Li, JC
    Zhang, KL
    [J]. NANOTECHNOLOGY, 2006, 17 (05) : 1520 - 1526
  • [4] Novel nanostructures of functional oxides synthesized by thermal evaporation
    Dai, ZR
    Pan, ZW
    Wang, ZL
    [J]. ADVANCED FUNCTIONAL MATERIALS, 2003, 13 (01) : 9 - 24
  • [5] Humidity sensing properties of ZnO nanoparticles synthesized by sol-gel process
    Erol, A.
    Okur, S.
    Comba, B.
    Mermer, Oe
    Arikan, M. C.
    [J]. SENSORS AND ACTUATORS B-CHEMICAL, 2010, 145 (01): : 174 - 180
  • [6] Synthesis and application of lead telluride nanoparticles for degrediation of organic pollution
    Gholamrezaei, Sousan
    Salavati-Niasari, Masoud
    Ghanbari, Davood
    [J]. JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2014, 20 (06) : 4000 - 4007
  • [7] A facile hydrothermal method for synthesis different morphologies of PbTe nanostructures
    Gholamrezaei, Sousan
    Salavati-Niasari, Masoud
    Ghanbari, Davood
    [J]. JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2014, 20 (05) : 3335 - 3341
  • [8] Surface roughness analysis and magnetic property studies of nickel thin films electrodeposited onto rotating disc electrodes
    Hedayati, K.
    Nabiyouni, G.
    [J]. APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 2014, 116 (04): : 1605 - 1612
  • [9] Synthesis, surface modification and photocatalytic property of ZnO nanoparticles
    Hong, R. Y.
    Li, J. H.
    Chen, L. L.
    Liu, D. Q.
    Li, H. Z.
    Zheng, Y.
    Ding, J.
    [J]. POWDER TECHNOLOGY, 2009, 189 (03) : 426 - 432
  • [10] Influence of solvent on the growth of ZnO nanoparticles
    Hu, ZS
    Oskam, G
    Searson, PC
    [J]. JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2003, 263 (02) : 454 - 460