NiO Nanoparticles: Synthesis and Characterization

被引：274
作者：
Rahdar, A. [1 ]
Aliahmad, M. [2 ]
Azizi, Y. [2 ]
机构：
[1] Univ Zabol, Dept Phys, Fac Sci, Zabol, Iran
[2] Univ Sistan & Baluchestan, Dept Phys, Fac Sci, Zahedan, Iran
来源：
JOURNAL OF NANOSTRUCTURES | 2015年 / 5卷 / 02期
关键词：
Precipitation method; NiO:Cu nanoparticles; Hysteresis loop; VSM;
D O I：
10.7508/jns.2015.02.009
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
In the current paper, Nanostructured Nickel oxide (NiO) were synthesized by co-precipitation method using Nickel(II) Chloride Hexahydrate (NiCl2 center dot 6H(2)O) and sodium hydroxide (NaOH) as starting material. Structural, optical and magnetic properties of nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Atomic force microscope (AFM), UV-Vis absorption; Fourier transformed infrared (FTIR) and vibrating sample magnetometer (VSM) technique. The X-ray diffraction pattern studies revealed the NiO have a face-centered cubic (FCC) structure and confirmed the presence of high degree of crystallinity nature NiO nanoparticles that their average size is found to be 26 nm. The composition of nanostructures confirmed by analysis of FTIR spectra. The average size of the NiO nanoparticle observed from scanning electron microscopy images is found to be dimensions about 24 nm. Magnetic measurement confirmed the Nickel Oxide nanostructures superparamagnetic behavior at room temperature (RT) after calcinations. 2015 JNS All rights reserved
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收藏
页码：145 / 151
页数：7
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