Facile Rapid Synthesis of Polyaniline (PANI) Nanofibers

被引：15
作者：
Bhagwat, Ashok D. [1 ,2 ]
Sawant, Sachin S. [1 ,3 ]
Mahajan, Chandrashekhar M. [3 ]
机构：
[1] Singhania Univ, Jhunjhunu 333515, Rajasthan, India
[2] Dnyanshree Inst Engn & Technol, Satara 415013, Maharashtra, India
[3] Vishwakarma Inst Technol, Dept Engn Sci & Humanities, Pune 411037, Maharashtra, India
来源：
JOURNAL OF NANO- AND ELECTRONIC PHYSICS | 2016年 / 8卷 / 01期
关键词：
Mesh; Nano-fibers; Polyaniline; Rapid mixing; Synthesis;
D O I：
10.21272/jnep.8(1).01037
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
A Polyaniline (PANI) nanofibers have been successfully synthesized by a facile rapid oxidative polymerization of aniline hydrochloride and ammonium persulfate at high temperature (60 degrees C). The structural and optical properties of PANI nanofibers are investigated by using X-ray diffraction (XRD), UV-VIS Spectroscopy and Fourier Transform Infrared Spectroscopy (FTIR). The XRD analysis ascertains formation of PANI with nanocrystalline nature with average crystallite size 30 nm. Further, FTIR pattern confirmed the formation of PANI. SEM analysis has revealed homogeneous fibrous morphology of PANI nanofibers, a well formed mesh of interconnected and entangled PANI nano-fibers over the scanned area. The UV-VIS spectroscopic analysis shows three major absorption peaks at 256.73, 361.17 and 480.95 nm confirmed the PANI formation with conducting state.
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页数：3
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