DETERMINATION OF UNSULPHONATED QUINOLINE YELLOW IN SOFT DRINKS BY SOLID-PHASE SPECTROPHOTOMETRY

被引：3
作者：
CAPITANVALLVEY, LF [1 ]
DEORBE, I [1 ]
LOPEZRODRIGUEZ, S [1 ]
AVIDAD, R [1 ]
机构：
[1] UNIV GRANADA,DEPT ANALYT CHEM,E-18071 GRANADA,SPAIN
来源：
MIKROCHIMICA ACTA | 1995年 / 117卷 / 3-4期
关键词：
QUINOLINE YELLOW DETERMINATION; QUINOLINE YELLOW SPIRIT SOLUBLE DETERMINATION; SOFT DRINKS ANALYSIS; SOLID-PHASE SPECTROPHOTOMETRY;
D O I：
10.1007/BF01244883
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A spectrophotometric method for determination of quinoline yellow spirit soluble (QYSS) in the presence of sulphonated quinoline yellow water soluble (QYWS) in soft drinks at trace levels is reported. The method is based on the fixation of QYSS on C-18 silica gel, followed by measurement of its absorbance at lambda = 418 nm in the solid phase after being packed in a 1-mm cell. The applicable concentration range was 1.5-15.0 ng/ml, the detection limit 0.4 ng/ml and the relative standard deviation 5.2%. The method was applied satisfactorily to the determination of this compound in samples of commercial soft drinks.
引用
收藏
页码：129 / 135
页数：7
相关论文
共 50 条
  • [41] Determination of Zinc in Environmental Samples by Solid Phase Spectrophotometry: Optimization and Validation Study
    Ma Francisca Molina
    Mounir Nechar
    Juan M. Bosque-Sendra
    Analytical Sciences, 1998, 14 : 791 - 797
  • [42] Determination of zinc in environmental samples by solid phase spectrophotometry: Optimization and validation study
    Molina, MF
    Nechar, M
    Bosque-Sendra, M
    ANALYTICAL SCIENCES, 1998, 14 (04) : 791 - 797
  • [43] Utilization of solid phase spectrophotometry for determination of trace amounts of beryllium in natural water
    Amin, AS
    ANALYTICA CHIMICA ACTA, 2001, 437 (02) : 265 - 272
  • [44] Solid-phase spectrophotometric and test determination of silicate in natural water
    Zaporozhets, Olga A.
    Bas, Julia P.
    Kachan, Igor A.
    Zinko, Lionel S.
    Davydov, Valentyn I.
    TALANTA, 2012, 90 : 85 - 90
  • [45] Design of Methodologies for the Determination of Selenium and Mercury in Samples of Environmental Interest by Solid Phase Spectrophotometry
    Shallal, Muhammed Abdel Hasan
    JOURNAL OF POPULATION THERAPEUTICS AND CLINICAL PHARMACOLOGY, 2023, 30 (03): : E373 - E384
  • [46] Utility of solid phase spectrophotometry for the modified determination of trace amounts of cadmium in food samples
    Amin, Alaa S.
    Gouda, Ayman A.
    FOOD CHEMISTRY, 2012, 132 (01) : 518 - 524
  • [47] Simple solid-phase spectrophotometric method for free iron(III) determination
    Alberti, Giancarla
    Emma, Giovanni
    Colleoni, Roberta
    Nurchi, Valeria Marina
    Pesavento, Maria
    Biesuz, Raffaela
    ARABIAN JOURNAL OF CHEMISTRY, 2019, 12 (04) : 573 - 579
  • [48] Solid-phase spectrophotometric determination of beryllium at ng mL-1
    Molina-Diaz, A
    Ayora-Canada, MJ
    Pascual-Reguera, MI
    SPECTROSCOPY LETTERS, 1998, 31 (03) : 503 - 520
  • [49] Design of Methodologies for the Determination of Selenium and Mercury in Samples of Environmental Interest by Solid Phase Spectrophotometry
    Shallal, Muhammed Abdel Hasan
    JOURNAL OF POPULATION THERAPEUTICS AND CLINICAL PHARMACOLOGY, 2023, 30 (03): : E373 - E384
  • [50] Solid-Phase Spectrophotometric Determination of Mercury(II) Ions Using Diphenylcarbazone
    Posvyashchennaya, A. K.
    Volgina, T. N.
    Gavrilenko, M. A.
    CHEMISTRY FOR SUSTAINABLE DEVELOPMENT, 2018, 26 (01): : 51 - 55
12345