Optimization of Microwave Process Parameters in Preparation of Ni-Fe Hydrotalcite by Response Surface Methodology and Evaluation of Photocatalytic Degradation of Antibiotic Wastewater

被引:4
作者
Niu, Jinfen [1 ,2 ]
Ma, Zhangtengfei [1 ]
Zhang, Yue [1 ]
Shi, Jiahui [1 ]
Yang, Lan [1 ]
Yao, Binghua [1 ,2 ]
Yu, Xiaojiao [1 ,2 ]
Wei, Hong [3 ]
机构
[1] Xian Univ Technol, Sch Sci, Xian, Peoples R China
[2] Xian Univ Technol, Res Ctr Micro&Nano Mat, Xian, Peoples R China
[3] Xian Univ Technol, State Key Lab Ecohydraul Northwest Arid Reg, Xian, Peoples R China
关键词
Response surface methodology; NiFe-LDH; photocatalytic degradation; microwave hydrothermal method; LDH; REMOVAL; CARBON; BLUE;
D O I
10.1080/10584587.2022.2072134
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Using the response surface method (RSM), the temperature, time and nickel-iron ratio of the synthesis of NiFe-LDH photocatalyst were used as influencing factors, the removal rate of norfloxacin (NOR) was the response factor, the Sub-mathematical equation was structured. The optimized model predicts that the optimal synthesis temperature, time and nickel-iron ratio are: 127.1 degrees C, 36 min, 2.854:1, and the removal rate of NOR is 88.25%. The actual removal rate of NOR over NiFe-LDH prepared under the conditions was 89.14%, indicating that the model was successfully established. It provides a reference for the synthesis of hydrotalcite by microwave method.
引用
收藏
页码:192 / 201
页数:10
相关论文
共 23 条
[11]   Optimization of the Process Variables for the Synthesis of Starch-Based Biodegradable Resin Using Response Surface Methodology [J].
Hong, Fu-Liang ;
Peng, Jinchyau ;
Lui, Wai-Bun .
JOURNAL OF APPLIED POLYMER SCIENCE, 2011, 119 (03) :1797-1804
[13]   Mechanochemical synthesis of novel Pt modified ZnAl-LDH for effective ciprofloxacin photodegradation [J].
Li, Zhao ;
Chen, Min ;
Hu, Huimin ;
Zhang, Qiwu ;
Tao, Dongping .
JOURNAL OF SOLID STATE CHEMISTRY, 2020, 290
[14]   Facile fabrication of NiAl-LDH and its application in TPU nanocomposites targets for reducing fire hazards [J].
Liu, Xinliang ;
Ge, Xiangtong ;
Liu, Mengru ;
Zhou, Keqing ;
Zhu, Qingming ;
Chen, Depeng ;
Liu, Chunlin ;
Wang, Changlong ;
Liu, Xiuyu ;
Tang, Gang .
PLASTICS RUBBER AND COMPOSITES, 2021, 50 (06) :285-298
[15]   Phenol contaminated water treatment by photocatalytic degradation on electrospun Ag/TiO2 nanofibers: Optimization by the response surface method [J].
Norouzi, Mahtab ;
Fazeli, Ali ;
Tavakoli, Omid .
JOURNAL OF WATER PROCESS ENGINEERING, 2020, 37
[16]   Microwave synthesis of histidine-functionalized graphene quantum dots/Ni-Co LDH with flower ball structure for supercapacitor [J].
Qiu, Hengrui ;
Sun, Xuejiao ;
An, Shengli ;
Lan, Dawei ;
Cui, Jinlong ;
Zhang, Yongqiang ;
He, Wenxiu .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2020, 567 :264-273
[17]   Electrochemical treatment of sugar industry wastewater: process optimization by response surface methodology [J].
Sahu, O. ;
Mazumdar, B. ;
Chaudhari, P. K. .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY, 2019, 16 (03) :1527-1540
[18]   Synthesis of advanced MgAl-LDH based geopolymer as a potential catalyst in the conversion of waste sunflower oil into biodiesel: Response surface studies [J].
Sayed, Maha R. ;
Abukhadra, Mostafa R. ;
Ahmed, Sayed Abdelkader ;
Shaban, Mohamed ;
Javed, Umer ;
Betiha, Mohamed A. ;
Shim, Jae-Jin ;
Rabie, Abdelrahman M. .
FUEL, 2020, 282
[19]   Atomically targeting NiFe LDH to create multivacancies for OER catalysis with a small organic anchor [J].
Wang, Yaqiong ;
Tao, Shi ;
Lin, He ;
Wang, Gaopeng ;
Zhao, Kangning ;
Cai, Rongmin ;
Tao, Kewen ;
Zhang, Chengxu ;
Sun, Mingzi ;
Hu, Jue ;
Huang, Bolong ;
Yang, Shihe .
NANO ENERGY, 2021, 81 (81)
[20]   Modification of abandoned fine blue-coke: optimization study on removal of p-nitrophenol using response surface methodology [J].
Wei, Fengyu ;
Wu, Bo ;
Zhang, Jincheng ;
Zhang, Wanting .
RSC ADVANCES, 2016, 6 (16) :13537-13547