EFFICIENT PROCEDURES FOR 1-BROMO-1,3-BUTADIENE AND 2-BROMO-1,3-BUTADIENE

被引：10

作者：

KEEGSTRA, MA ^{[1
]}

VERKRUIJSSE, HD ^{[1
]}

ANDRINGA, H ^{[1
]}

BRANDSMA, L ^{[1
]}

机构：

[1] UNIV UTRECHT,DEBIJE INST,DEPT PREPARAT ORGAN CHEM,PADUALAAN 8,3584 CH UTRECHT,NETHERLANDS

来源：

SYNTHETIC COMMUNICATIONS | 1991年 / 21卷 / 05期

关键词：

D O I：

10.1080/00397919108020841

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Mixtures of Z- and E-1-bromo-1,3-butadiene in which the E- or Z- isomer predominates have been obtained in good yields by treating a mixture of Z- and E-1,4-dibromo-2-butene (90% Z-isomer) or pure E-1,4-dibromo-2-butene, respectively, with powered potassium hydroxide in high-boiling petroleum. 2-Bromo-1,3-butadiene was obtained in high yields by stirring a mixture of vinylacetylene, concentrated aqueous hydrogen bromide and copper(I) bromide.

引用

页码：721 / 726

页数：6

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