TRIMETHYLSILYLATION - AID IN NMR ANALYSIS OF OLIGOSACCHARIDES - ASSIGNMENT OF SI-29 AND C-13 NMR-SPECTRA OF TRIMETHYLSILYATED METHYL BETA-D-XYLOBIOSIDES BY 2D NMR

被引:11
作者
SCHRAML, J
PETRAKOVA, E
PELNAR, J
KVICALOVA, M
CHVALOVSKY, V
机构
[1] SLOVAK ACAD SCI, INST CHEM, CS-84238 BRATISLAVA, CZECHOSLOVAKIA
[2] CZECHOSLOVAK ACAD SCI, INST ORGAN CHEM & BIOCHEM, CS-16610 PRAGUE 6, CZECHOSLOVAKIA
关键词
D O I
10.1080/07328308508070189
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
引用
收藏
页码:393 / 403
页数:11
相关论文
共 18 条
[1]  
BAX A, 1982, 2 DIMENSIONAL NUCLEA, P50
[2]  
BREVARD C, 1982, HDB HIGH RESOLUTION, P100
[3]  
CHAMBAZ EM, 1967, ANAL LETT, V1, P201
[4]  
CHAMBAZ EM, 1967, ANAL LETT, V1, P749
[5]   DISTORTIONLESS ENHANCEMENT OF NMR SIGNALS BY POLARIZATION TRANSFER [J].
DODDRELL, DM ;
PEGG, DT ;
BENDALL, MR .
JOURNAL OF MAGNETIC RESONANCE, 1982, 48 (02) :323-327
[6]   SI-29 AND C-13 NMR-STUDIES OF ORGANOSILICON CHEMISTRY .5. SUGAR DERIVATIVES [J].
GALE, DJ ;
HAINES, AH ;
HARRIS, RK .
ORGANIC MAGNETIC RESONANCE, 1975, 7 (12) :635-636
[7]   SI-29 AND C-13 NMR-STUDIES OF ORGANOSILICON CHEMISTRY .8. ASSIGNMENT OF SI-29 AND RELATED H-1 RESONANCES OF TRIMETHYLSILYLATED SUGARS BY DEUTERATION AND SHIFT-REAGENT STUDIES [J].
HAINES, AH ;
HARRIS, RK ;
RAO, RC .
ORGANIC MAGNETIC RESONANCE, 1977, 9 (07) :432-437
[9]   ENHANCEMENT OF NUCLEAR MAGNETIC-RESONANCE SIGNALS BY POLARIZATION TRANSFER [J].
MORRIS, GA ;
FREEMAN, R .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1979, 101 (03) :760-762
[10]  
PAST J, COLLECT CZECH CHEM C