LOW-TEMPERATURE STABILIZATION OF PURE NI(II)O

被引：2
作者：
NANJUNDASWAMY, KS
MURTHY, MNS
机构：
[1] Indian Inst of Science, Bangalore, India, Indian Inst of Science, Bangalore, India
来源：
MATERIALS CHEMISTRY AND PHYSICS | 1986年 / 15卷 / 01期
关键词：
MICROSCOPIC EXAMINATION - Specimen Preparation;
D O I：
10.1016/0254-0584(86)90087-8
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Ordinary nickel (II) prepared by any of the usual methods is always contaminated with some higher valency states of nickel. Such nickel oxide however can be converted to pure nickel (II) oxide by soaking for some hours at 800-850 degree C in a closed system under a static inert atmosphere and in the presence of pure MnO as oxygen-getter. The resulting Ni(II)O is highly resistant to oxidation.
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页码：37 / 44
页数：8
相关论文
共 9 条
  • [1] SURFACE REDUCTION OF SOME TRANSITION-METAL OXIDES - AN X-RAY PHOTOELECTRON SPECTROSCOPIC STUDY OF IRON, COBALT, NICKEL AND ZINC-OXIDES
    COCHRAN, SJ
    LARKINS, FP
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS I, 1985, 81 : 2179 - 2190
  • [2] DUVAL C, 1963, INORGANIC THERMOGRAV, P355
  • [3] INITIAL-STAGES OF HYDROGEN REDUCTION OF NIO(100)
    FURSTENAU, RP
    MCDOUGALL, G
    LANGELL, MA
    [J]. SURFACE SCIENCE, 1985, 150 (01) : 55 - 79
  • [4] Glemser O., 1965, HDB PREPARATIVE INOR, V2, P1548
  • [5] HAYWARD DO, 1964, CHEMISORPTION, P85
  • [6] X-RAY PHOTOELECTRON SPECTROSCOPIC STUDIES OF NICKEL-OXYGEN SURFACES USING OXYGEN AND ARGON ION-BOMBARDMENT
    KIM, KS
    WINOGRAD, N
    [J]. SURFACE SCIENCE, 1974, 43 (02) : 625 - 643
  • [7] Nanjundaswamy K. S., 1985, Bulletin of Materials Science, V7, P459, DOI 10.1007/BF02744055
  • [8] PHASE-RELATIONS IN THE LA-NI-O SYSTEM - INFLUENCE OF TEMPERATURE AND STOICHIOMETRY ON THE STRUCTURE OF LA2NIO4
    ODIER, P
    NIGARA, Y
    COUTURES, J
    SAYER, M
    [J]. JOURNAL OF SOLID STATE CHEMISTRY, 1985, 56 (01) : 32 - 40
  • [9] SCHENK PW, 1963, HDB PREPARATIVE INOR, V1, P458
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