A N-15, C-13, AND H-1-NMR STUDY OF REACTION-PRODUCTS FROM ARYLGUANIDINES AND CHLOROFORMATE ESTERS

被引：2

作者：

LYCKA, A ^{[1
]}

PALAT, K ^{[1
]}

机构：

[1] CHARLES UNIV, FAC PHARM, CS-50165 HRADEC KRALOVE, CZECHOSLOVAKIA

来源：

COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS | 1991年 / 56卷 / 07期

关键词：

D O I：

10.1135/cccc19911505

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The N-15, C-13, and H-1 NMR spectra of the reaction products from arylguanidines with two mols of chloroformate esters have been measured. With application of the corresponding N-15 isotopomer it has been proved that the reaction products have the structures IIIa-IIIo.

引用

页码：1505 / 1511

页数：7

共 8 条

[1] STRUCTURE DETERMINATION AND SPECTRAL ASSIGNMENT BY PULSED POLARIZATION TRANSFER VIA LONG-RANGE H-1-C-13 COUPLINGS [J].

BAX, A .

JOURNAL OF MAGNETIC RESONANCE, 1984, 57 (02) :314-318

[2]

Ernst R. R., 1987, PRINCIPLES NUCL MAGN, V1st

[3] C-13 SUBSTITUENT EFFECTS IN MONOSUBSTITUTED BENZENES [J].

EWING, DF .

ORGANIC MAGNETIC RESONANCE, 1979, 12 (09) :499-524

[4]

KLOPPING HL, 1960, Patent No. 2933504

[5] The action of amines on the esters of carboxy substituted ureas, thioureas and guanidines III [J].

Murray, JA ;

Dains, FB .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1934, 56 :144-146

[6]

PALAT K, IN PRESS CEXK FARM

[7]

WOLLWEBER H, 1984, ARZNEIMITTEL-FORSCH, V34-1, P531

[8]

WUNSCH E, 1974, METHODEN ORGANISCHEN, V15, pCH36

← 1 →