THERMAL-DEGRADATION PRODUCTS OF A N,N-DIALKYLAMIDE - IDENTIFICATION BY GC/EI-MS, GC/CI-MS AND GC/FTIR

被引：0

作者：

DAGNAC, T

GUILLOT, JM

ROULPH, C

LECLOIREC, P

CHARBONNEL, MC

机构：

[1] ECOLE MINES ALES,GENIE ENVIRONM IND LAB,F-30319 ALES,FRANCE

[2] CEA,CE VALRHO MARCOULE,DRDD,SEMP,GEA,F-30205 BAGNOLS SUR CEZE,FRANCE

来源：

ANALUSIS | 1995年 / 23卷 / 03期

关键词：

THERMAL DEGRADATION; N; N-DIALKYLAMIDE; MASS SPECTROMETRY; FOURIER TRANSFORM INFRARED SPECTROSCOPY; EXTRACTANT;

D O I：

暂无

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Due to their utilization in the nuclear process, the N,N-dialkylamides' thermal stability must be well known. The degradation of such a compound has been studied in a temperature range of 175 to 255 degrees C under different atmospheres. The degradation mixture was separated by gas chromatography (GC) and the structural characterization of the 15 major products was ensured by the combined application of Fourier transform infrared spectroscopy (FTIR) and mass spectrometry (MS).

引用

页码：120 / 124

页数：5

共 13 条

[1] PYROLYSIS OF ESTERS .13. PYROLYSIS OF AMIDES [J].