3,3',5,5'-Tetra-tert-butyl-2'-hydroxy[1,1'biphenyl]-2-yl 4-methylbenzene-sulfonate

被引:0
作者
Jian, Chunli [1 ]
Zhang, Jinjin [1 ]
Wang, Lei [1 ]
Tang, Ning [1 ]
Wu, Jincai [1 ]
机构
[1] Lanzhou Univ, Dept Chem, Lanzhou 730000, Peoples R China
基金
中国国家自然科学基金;
关键词
single-crystal X-ray study; T = 296 K; mean sigma(C-C) = 0.005 A(degrees); disorder in main residue; R factor = 0.074; wR factor = 0.205; data-to-parameter ratio = 19.6;
D O I
10.1107/S1600536812051938
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title molecule, C37H48O4S, the benzene rings in the biphenyl fragment are inclined to each other at 61.1 (1)(degrees). The hydroxy group is involved in a weak intramolecular O-H...O-sulfonate hydrogen bond. One tert-butyl group is disodered over two orientations in a 0.682 (17): 0.318 (17) ratio. In the crystal, weak C-H...O hydrogen bonds link the molecules into columns in direction [100].
引用
收藏
页码:O186 / +
页数:12
相关论文
共 5 条
[1]  
Bruker, 2004, SAINT SADABS
[2]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[3]   2,4-Di-tert-butyl-6-[(R/S)-1-(3,5-di-tert-butyl-2-hydroxyphenyl)ethyl]phenyl [(1R,4S)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl]methanesulfonate [J].
Wang, Cheng ;
Wu, Jincai .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :O93-U198
[4]   Recent developments in main group metal complexes catalyzed/initiated polymerization of lactides and related cyclic esters [J].
Wu, JC ;
Yu, TL ;
Chen, CT ;
Lin, CC .
COORDINATION CHEMISTRY REVIEWS, 2006, 250 (5-6) :602-626
[5]   2,4-Di-tert-butyl-6-[1-(3,5-di-tert-butyl-2-hydroxyphenyl)ethyl]phenyl 4-methylbenzenesulfonate [J].
Wu, Jincai ;
Pan, Xiaobo ;
Wang, Lei ;
Yao, Lihui .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O155-U2615