Synthesis and characterization of ZnO-CuO nanocomposites powder by modified perfume spray pyrolysis method and its antimicrobial investigation

被引:159
作者
Saravanakkumar, D. [1 ,6 ]
Sivaranjani, S. [1 ,2 ]
Kaviyarasu, K. [3 ,4 ]
Ayeshamariam, A. [1 ,5 ]
Ravikumar, B. [6 ]
Pandiarajan, S. [6 ]
Veeralakshmi, C. [6 ]
Jayachandran, M. [7 ]
Maaza, M. [3 ,4 ]
机构
[1] Bharathiyar Univ, Res & Dev Ctr, Coimbatore 641046, Tamil Nadu, India
[2] SBM Coll Engn & Technol, Dept Phys, Dindigul 624001, India
[3] Univ South Africa UNISA, Coll Grad Studies, UNESCO UNISA Africa Chair Nanosci Nanotechnol Lab, Pretoria, South Africa
[4] Natl Res Fdn, iThemba LABS, MRG, Nanosci African Network NANOAFNET, Somerset West, Western Cape Pr, South Africa
[5] Khadir Mohideen Coll, Dept Phys, Adirampattinam 614701, India
[6] Devanga Arts Coll, Dept Phys, Aruppukkottai 626101, India
[7] Sethu Inst Technol, Dept Phys, Pullor 626115, Kariapatti, India
关键词
MSP method; XRD; FTIR; FESEM; CuO nanoparticles;
D O I
10.1088/1674-4926/39/3/033001
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Pure ZnO, ZnO-CuO nanocomposites can be synthesized by using a modified perfume spray pyrolysis method (MSP). The crystallite size of the nanoparticles (NPs) has been observed by X-ray diffraction pattern and is nearly 36 nm. Morphological studies have been analyzed by using Field Emission Scanning Electron Microscopy (FESEM) and its elemental analysis was reported by Elemental X-ray Analysis (EDX); these studies confirmed that ZnO and CuO have hexagonal structure and monoclinic structure respectively. Fourier Transform Infrared (FTIR) spectra revealed that the presence of functional frequencies of ZnO and CuO were observed at 443 and 616 cm(-1). The average bandgap value at 3.25 eV using UV-vis spectra for the entitled composite has described a blue shift that has been observed here. The antibacterial study against both gram positive and negative bacteria has been studied by the disc diffusion method. To the best of our knowledge, it is the first report on ZnO-CuO nanocomposite synthesized by a modified perfume spray pyrolysis method.
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页数:7
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