X-RAY CRYSTAL-STRUCTURE OF 2,4,6-TRIS(PARA-METHOXYPHENYL)-1,3,5,2,4,6-TRIOXATRIPHOSPHINANE 2,4,6-TRISULFIDE, A CO-PRODUCT IN P = O -] P = S THIONATION WITH LAWESSON REAGENT

被引：11

作者：

WEN, T ^{[1
]}

BAU, R ^{[1
]}

MCKENNA, CE ^{[1
]}

机构：

[1] UNIV SO CALIF,DEPT CHEM,LOS ANGELES,CA 90089

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1991年 / 17期

关键词：

D O I：

10.1039/c39910001223

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

2,4,6-Tris(p-methoxyphenyl)-1,3,5,2,4,6-trioxatriphosphinane 2,4,6-trisulphide 2, obtained from trimethyl phosphonoformate ester 3 and Lawesson's reagent 1 in acetonitrile, has been structurally characterized by X-ray diffraction.

引用

页码：1223 / 1224

页数：2

共 50 条

[1] SYNTHESIS AND CHARACTERIZATION OF STERICALLY HINDERED DIARYLSILANES CONTAINING 2,4,6-TRIMETHYLPHENYL AND 2,4,6-TRIS(TRIFLUOROMETHYL)PHENYL SUBSTITUENTS, X-RAY CRYSTAL-STRUCTURE OF BIS[2,4,6-TRIS(TRIFLUOROMETHYLPHENYL)]FLUOROSILANE
BRADDOCKWILKING, J
SCHIESER, M
BRAMMER, L
HUHMANN, J
SHALTOUT, R
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1995, 499 (1-2) : 89 - 98
[2] Synthesis and characterization of sterically hindered diarylsilanes containing 2,4,6-trimethylphenyl and 2,4,6-tris(trifluoromethyl) phenyl substituents. X-ray crystal structure of bis[2,4,6-tris(trifluoromethylphenyl)]fluorosilane
Braddock-Wilking, J.
Schieser, M.
Brammer, L.
Huhmann, J.
1600, (499): : 1 - 2
[3] SYNTHESIS AND CRYSTAL-STRUCTURE OF 2,4,6-TRIFERROCENYL-1,3,5,2,4,6-TRISELENATRIBORINANE
HORN, H
RUDOLPH, F
AHLRICHS, R
MERZWEILER, K
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1992, 47 (01): : 1 - 4
[4] Crystal structure of 2,4,6-tris(cyclohexyloxy)-1,3,5-triazine
Sankolli, Ravish
Hauser, Juerg
Row, T. N. Guru
Hulliger, Juerg
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 1328 - +
[5] SYNTHESIS OF PLATINUM COMPLEXES OF 2-METHYL-2,4,6-TRIS(TRIFLUOROMETHYL)-PYRAN - X-RAY CRYSTAL-STRUCTURE OF (CYCLO-OCTA-1,5-DIENE)[2-METHYL-2,4,6-TRIS(TRIFLUOROMETHYL)PYRAN]PLATINUM
CHRISTOFIDES, A
HOWARD, JAK
RATTUE, JA
SPENCER, JL
STONE, FGA
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1980, (11): : 2095 - 2101
[6] CHEMISTRY OF SILYL THIOKETONES .4. 2,4,6-TRIARYL-2,4,6-TRIS(TRIMETHYLSILYL)-1,3,5-TRITHIANES FROM SILYL THIOKETONES - CRYSTAL-STRUCTURE OF 2,4,6-TRIPHENYL-2,4,6-TRIS(TRIMETHYLSILYL)-1,3,5-TRITHIANE AND STEREOCHEMISTRY OF DESILYLATION WITH FLUORIDE-ION
BONINI, BF
MAZZANTI, G
ZANI, P
MACCAGNANI, G
FORESTI, E
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1988, (06): : 1499 - 1502
[7] SYNTHESIS AND NUCLEAR MAGNETIC-RESONANCE SPECTROSCOPY OF GEOMETRICAL-ISOMERS OF 1,3,5-TRIMETHYL-2,4,6-TRIS(PARA-METHYLPHENOXY)-2,4,6-TRIOXOCYCLOTRIPHOSPHAZANE - X-RAY CRYSTAL-STRUCTURE OF THE TRANS ISOMER
KARTHIKEYAN, S
VYAS, K
KRISHNAMURTHY, SS
CAMERON, TS
VINCENT, BR
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1988, (05): : 1371 - 1375
[8] Synthesis, structure and optical properties of 2,4,6-tris(p-methylstyryl)-s-triazine
Cui, YZ
Fang, Q
Xue, G
Yu, WT
Lei, H
Cheng, XF
Zhang, SJ
Liu, GQ
ACTA CHIMICA SINICA, 2004, 62 (06) : 620 - 624
[9] 2,4,6-TRIS(2,6-DI-TERT-BUTYL-4-SUBSTITUTED-PHENOXY)-1,3,5,2,4,6-TRIOXATRIPHOSPHORINANES - SYNTHESIS, CHARACTERIZATION, X-RAY STRUCTURE, AND SOLID-STATE P-31 NMR OF A NOVEL FAMILY OF PHOSPHORUS(III)-OXYGEN HETEROCYCLES
CHASAR, DW
FACKLER, JP
MAZANY, AM
KOMOROSKI, RA
KROENKE, WJ
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1986, 108 (19) : 5956 - 5962
[10] CRYSTAL AND MOLECULAR STRUCTURE OF HEXAMETHYLMELAMINE [2,4,6-TRIS(DIMETHYLAMINO)-1,3,5-TRIAZINE]
BULLEN, GJ
STEPHENS, FS
CORNEY, DJ
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1972, (05): : 642 - &

← 1 2 3 4 5 →