New dibenzocyclooctadiene lignan from Schisandra chinensis (Turcz.) Baill. fruits

被引：0
|
作者：
Trong Nguyen Nguyen
Yeong-Geun Lee
Hyoung-Geun Kim
Dahye Yoon
Jin Tae Jeong
Dae Young Lee
Nam-In Baek
机构：
[1] KyungHee University,Graduate School of Biotechnology
[2] National Institute of Horticultural and Herbal Science,Department of Herbal Crop Research
[3] RDA,undefined
来源：
Applied Biological Chemistry | 2021年 / 64卷
关键词：
Atropisomer; Axial chirality; Circular dichroism; Dibenzocyclooctadiene lignan; Gomisin M3;
D O I：
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摘要：
Repeated column chromatography using Sephadex LH-20, silica gel (SiO2), and octadecyl SiO2 (ODS) as well as preparative HPLC column chromatography led to isolation of a new dibenzocyclooctadiene lignan along with four known ones, gomisin L2 (1), L1 (2), M1 (3), and M2 (4). Their chemical structures were fixed based on MS, IR, and NMR data analyses. In addition, the stereochemistry of atropisomers, the absolute configuration of the axial chirality in a biphenyl structure, was confirmed by a CD experiment. The new lignan was named gomisin M3 (5).
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