Synthesis and Crystal Structure of 5,7,12,13b,13c,14-Hexahydro-1,4,-dibromo-8,11-dimethoxy-13b,13c-bis(ethoxycarbonyl)-6H,13H-5a,6a,12a,13a-tetra azbenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

被引：0
作者：
Zhiguo Wang
Yuzhou Wang
Guodong Yin
Anxin Wu
机构：
[1] Ministry of Education,Key Lab of Pesticide & Chemical Biology
[2] Chemistry Department of Central China Normal University,School of Chemical and Materials Engineering
[3] Huangshi Institute of Technology,undefined
来源：
Journal of Chemical Crystallography | 2008年 / 38卷
关键词：
Crystal structure; Supramolecule; Dimeric aggregates; Hydrogen bond; π–π stacking;
D O I：
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中图分类号：
学科分类号：
摘要：
The title compound has been synthesized by the reaction of 4 with 1,4-dimethoxybenzene. The yielded product 5 was investigated with X-ray crystallographic, NMR, EI-MS, and IR techniques. The crystal belongs to a monoclinic system, space group P21/c with unit cell parameters a = 12.7790(17) Å, b = 21.565(3) Å, c = 12.2544(16) Å, α = 90°, β = 107.014(2)°, γ = 90°, V = 3229.3(7) Å3, Z = 4, Dc = 1.661, Mr = 807.32, μ = 2.732 mm−1, F(000) = 1632, R1 = 0.0540 and wR2 = 0.0989.
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页码：591 / 594
页数：3
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