Crystal structure and spectroscopic characterization of bis(N-phenylthiourea)

被引：0
作者：
Narayan T. Akinchan
Piotr M. Drożdżewski
Luigi P. Battaglia
机构：
[1] University of Calabar,Department of Chemistry
[2] Wrocław University of Technology,Institute of Inorganic Chemistry and Metallurgy of Rare Elements
[3] University of Parma,undefined
来源：
Journal of Chemical Crystallography | 2002年 / 32卷
关键词：
Bis(; -phenylthiourea); crystal structure; IR; Raman; UV-Vis; H NMR; FAB;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Bis(N-phenylthiourea) (BPTU) has been synthesized and characterized by means of X-ray, IR, Raman, UV-Vis, 1H NMR, and FAB mass spectra. The BPTU crystal belongs to the monoclinic C2/c space group with the cell constants a = 26.992(8) Å, b = 6.336(3) Å, c = 9.463(3) Å, α = γ = 90°, β = 105.97(7)°, Z = 4. The compound has been found to exist in the thione form, with cis configuration of the thiosemicarbazone moiety and skew conformation of the molecule.
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页码：91 / 97
页数：6
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