Zinc aluminate (ZnAl2O4) applied in the development of a propane gas sensor and in the design of a digital gas detector

被引:0
作者
José Trinidad Guillen Bonilla
Alex Guillen Bonilla
Antonio Casillas Zamora
Héctor Guillen Bonilla
机构
[1] Universidad de Guadalajara,Departamento de Electro
[2] Universidad de Guadalajara,Fotónica, C.U.C.E.I.
[3] CUCEI University of Guadalajara,Departamento de Ciencias Computacionales e Ingenierías, Centro Universitario de los Valles (CUValles)
来源
Journal of Materials Science: Materials in Electronics | 2023年 / 34卷
关键词
D O I
暂无
中图分类号
学科分类号
摘要
When a propane gas sensor is developed based on a synthesized material, the goal is to use it in the development of new prototypes, which are applied in health and safety. In this work, zinc aluminate powders (ZnAl2O4) were synthesized using the colloidal method assisted with microwave radiation. The powders were characterized by X-ray diffraction, SEM, and TEM microscopy. With the diffraction analysis, the crystalline phase of the ZnAl2O4 oxide was demonstrated and with the electron microscopy images, the morphology of the particles was analyzed. In addition, based on these images, the particle size of the compound was estimated. With the calcined powders at 200 °C of ZnAl2O4, pellets were manufactured and electrically characterized (dynamic electrical tests) in atmospheres of dynamic propane at 200 °C, obtaining changes in electrical resistance as a function of time. The dynamic concentration of propane (1000 ppm) greatly influenced the excellent dynamic response in these operating conditions. Based on the electrical response of the sensor (ZnAl2O4), a first-order mathematical model was proposed and this was used to corroborate the stability of the sensor, its response to frequency and it was evaluated at 3s in order to estimate the resistance of the sensor Rpt\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$${R}_{p}\left(t\right)$$\end{document} when the sensor is exposed to propane gas. With the result obtained from resistance Rptt=3\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$${\left.{R}_{p}\left(t\right)\right|}_{t=3}$$\end{document}, a prototype gas detector was designed based on the PIC16F887A microcontroller whose characteristics are: operating temperature of 200 °C, 1000 ppm operating concentration, 3s response time, 5 V supply voltage, 110 V alarm signal, optocoupler protection circuit, easy operation and easy repair. Our prototype has practical application in industries where high temperature safety systems are required, for example: boiler chimneys and heat exchangers.
引用
收藏
相关论文
共 274 条
  • [1] Norizan MN(2022)undefined Nanomater 12 2278-633
  • [2] Abdullah N(2018)undefined Sens. Actuators B Chem. 277 604-157
  • [3] Halim NA(2022)undefined Chemosensors 10 57-18283
  • [4] Ngah SZ(2021)undefined Sens. Actuators B Chem. 341 130015-58
  • [5] Mohamad IS(2019)undefined Appl. Phys. A 125 883-690
  • [6] Gao X(2021)undefined Sensors 21 8462-46
  • [7] Zhang T(2017)undefined Sens. Actuators B Chem. 240 148-217
  • [8] Dadkhah M(2022)undefined J. Mater. Sci. Mater. 33 18268-12
  • [9] Tulliani JM(2012)undefined Appl. Surf. Sci. 261 52-7386
  • [10] Qin W(2012)undefined Sens. Actuators B Chem. 171–172 686-2955