Investigation of the products of interaction of cyclic diketones with nitrogen-containing 1,4-binucleophiles

被引:1
作者
Kolos N.N. [1 ]
Yurchenko E.N. [1 ]
Orlov V.D. [1 ]
Shishkina S.V. [1 ]
Shishkin O.V. [1 ]
机构
[1] Kharkov V. N. Karazin Natl. Univ.
关键词
Arylbis(5,5-dimethylcyclohexane-1,3-dion-2-yl)methanes; Cyclocondensation; Decahydroacridine-1,8-diones; Dimedone; Hexahydrodibenzo[b,e]-1,4-diazepin-1-ones; o-aminophenol; o-phenylenediamine;
D O I
10.1007/s10593-005-0098-3
中图分类号
学科分类号
摘要
The interaction of arylbis(5,5-dimethylcyclohexane-1,3-dion-2-yl)methanes with o-phenylenediamine and o-aminophenol leads to the preparation of 3,3-dimethyl-11-aryl-2,3,4,5,10,11-hexahydrobenzo[b,e]-1,4-diazepin-1-ones and 3,3,6,6-tetramethyl-9-aryl-10-(2-hydroxyphenyl)-2,4,5,7,9-decahydroacridine-1, 8-diones respectively. A one-pot method is proposed for the synthesis of derivatives of hexahydrodibenzo[b,e]-1,4-diazepin-1-ones. The structure of the first member of this series was confirmed by X-ray diffraction analysis. ©2004 Springer Science+Business Media, Inc.
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页码:1550 / 1559
页数:9
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