Reaction of N,N′-bis(trimethylsilyl)dicyandiamide with bis(η5-cyclopentadienylvanadium) dichloride

被引：0
|
作者：
A. S. Gordetsov
S. V. Zimina
S. V. Saprykina
L. B. Loginova
A. V. Piskunov
V. F. Ur’yash
E. M. Moseeva
机构：
[1] Nizhnii Novgorod State Medical Academy,
来源：
Russian Journal of General Chemistry | 2011年 / 81卷
关键词：
Differential Thermal Analysis; General Chemistry; Melamin; Trimethylsilyl; Cyanamide;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
1,3,5-Tris[bis(η5-cyclopentadienyl)chlorovanadium]melamin is prepared in high yield by the reaction of N,N′-bis(trimethylsilyl)dicyandiamide with bis(η5-cyclopentadienylvanadium) dichloride in tetrahydrofuran. As side products, trimethylchlorosilane and cyclopentadiene formed. Reaction of N,N′-bis(trimethylsilyl) dicyandiamide with benzoyl chloride results in the formation of tris(benzoyl)melamin.
引用
收藏
页码：658 / 662
页数：4
相关论文
共 37 条
  • [1] Reaction of N,N′-bis(trimethylsilyl)dicyandiamide with bis(η5-cyclopentadienylvanadium) dichloride
    Gordetsov, A. S.
    Zimina, S. V.
    Saprykina, S. V.
    Loginova, L. B.
    Piskunov, A. V.
    Ur'yash, V. F.
    Moseeva, E. M.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2011, 81 (04) : 658 - 662
  • [2] Reaction of N,N′-bis(trimethylsilyl)-N-methyl-N′-arylureas with chloro(chloromethyl)dimethylsilane
    Pudovik, MA
    Kibardina, LK
    Pudovik, AN
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2004, 74 (06) : 971 - 972
  • [3] Reaction of N,N'-Bis(trimethylsilyl)-N-methyl-N'-arylureas with Chloro(chloromethyl)dimethylsilane
    M. A. Pudovik
    L. K. Kibardina
    A. N. Pudovik
    Russian Journal of General Chemistry, 2004, 74 : 971 - 972
  • [4] 9-Trimethylsilyl-N,N-bis(trimethylsilyl)adenine
    Gostevskii, B. A.
    Albanov, A. I.
    Lazareva, N. F.
    RUSSIAN CHEMICAL BULLETIN, 2024, 73 (03) : 743 - 745
  • [5] A PREPARATION OF N,N-BIS(TRIMETHYLSILYL)ALLENAMINES
    CUNICO, RF
    KUAN, CP
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1995, 487 (1-2) : 89 - 93
  • [6] Application of N,N′-bis(trimethylsilyl)carbodiimide in the synthesis of new heterocyclic compounds
    Kirilin, A. D.
    Gavrilova, A. V.
    Shamina, M. G.
    Lakhtin, V. G.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2012, 82 (05) : 944 - 945
  • [7] Application of N,N′-bis(trimethylsilyl)carbodiimide in the synthesis of new heterocyclic compounds
    A. D. Kirilin
    A. V. Gavrilova
    M. G. Shamina
    V. G. Lakhtin
    Russian Journal of General Chemistry, 2012, 82 : 944 - 945
  • [8] Reactions of N,N'-Dimethyl-N,N'-bis(trimethylsilyl)methylphosphonic Diamide with Chloral and Chloromethyldimethylchlorosilane
    M. A. Pudovik
    L. K. Kibardina
    T. A. Zyablikova
    A. N. Pudovik
    Russian Journal of General Chemistry, 2001, 71 : 327 - 329
  • [9] Reactions of N,N′-dimethyl-N,N′-bis(trimethylsilyl)methylphosphonic diamide with chloral and chloromethyldimethylchlorosilane
    Pudovik, MA
    Kibardina, LK
    Zyablikova, TA
    Pudovik, AN
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2001, 71 (03) : 327 - 329
  • [10] Reaction of sodium bis(trimethylsilyl)amide with bromotoluenes
    A. V. Lis
    I. P. Tsyrendorzhieva
    A. I. Albanov
    B. A. Shainyan
    V. I. Rakhlin
    Russian Journal of Organic Chemistry, 2015, 51 : 335 - 340
1234