New Synthesis Method of N-Monosubstituted Ammonium-closo-Decaborates

被引：0

作者：

A. P. Zhdanov

V. V. Voinova

I. N. Klyukin

A. S. Kubasov

K. Yu. Zhizhin

N. T. Kuznetsov

机构：

[1] Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences,

[2] Lobachevsky State University of Nizhni Novgorod,undefined

来源：

Journal of Cluster Science | 2019年 / 30卷

关键词：

Nitrilium derivative; Boron cluster; -decaborate; Reduction process;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

In work, the process of interaction of nitrilium derivatives of the closo-decaborate anion with lithium aluminum hydride was studied. Reduction process proceeds under mild conditions and leads to the formation of N-alkylammonium-closo-decaborate with high yields and selectivity. For the structure of (NnBu4)[2-B10H9NH2CH2CH3] was confirmed by single-crystal X-ray diffraction.

引用

页码：1327 / 1333

页数：6

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