Inclusion complex of Isatoic anhydride with β-cyclodextrin and supramolecular one-pot synthesis of 2, 3-dihydroquinazolin-4(1H)-ones in aqueous media

被引：0
作者：
Dipak R. Patil
Pravin G. Ingole
Kripal Singh
Dipak S. Dalal
机构：
[1] North Maharashtra University,Department of Organic Chemistry
[2] Council of Scientific and Industrial Research (CSIR),Central Salt and Marine Chemicals Research Institute
来源：
Journal of Inclusion Phenomena and Macrocyclic Chemistry | 2013年 / 76卷
关键词：
-Cyclodextrin; Isatoic anhydride; Inclusion complex; IR spectroscopy; X-ray diffraction; Differential scanning calorimetry;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The inclusion complex of isatoic anhydride with β-cyclodextrin was formed as a result of intermolecular interaction between isatoic anhydride with β-CD. The inclusion complex was confirmed by IR spectroscopy, X-ray diffraction and DSC studies. From application of complex, herein we have described a simple and efficient protocol for synthesis of 2, 3-dihydroquinazoline-4(1H)-one derivatives by one pot condensation of isatoic anhydride, ammonium acetate or amine and aldehyde using β-CD as a supramolecular catalyst in aqueous media.
引用
收藏
页码：327 / 332
页数：5
相关论文
共 132 条
  • [1] Breslowong R(1998)Biomimetic reactions catalyzed by cyclodextrins and their derivatives Chem. Rev. 98 1997-2011
  • [2] Dong SD(1994)Catalysis of intramolecular aldol condensation by imidazole bearing cyclodextrin J. Am. Chem. Soc. 116 12081-12082
  • [3] Desper JM(1998)Introduction and general overview of cyclodextrin chemistry Chem. Rev. 98 1743-1754
  • [4] Breslow R(2007)Beta cyclodextrin as a catalyst in organic synthesis Min. Rev. Org. Chem. 4 143-157
  • [5] Szejtli J(1984)Application of isatoic anhydride chemistry to the synthesis of racemic paraensine J. Heterocyl. Chem. 21 1409-1410
  • [6] Bhosale SV(1944)Isatoic anhydride I reaction with primary and secondary amines and with some amides J. Org. Chem. 9 55-67
  • [7] Bhosale SV(1981)Isatoic anhydride and their uses in heterocyclic synthesis Adv. Heterocly. Chem. 28 127-182
  • [8] Coppola GM(2008)Novel quinazolinone derivatives as 5-HT Bioorg. Med. Chem. 16 2570-2578
  • [9] Schuster HF(1990) receptor ligands J. Med. Chem. 33 161-166
  • [10] Clark RH(2006)Synthesis and anticonvulsant activity of some new 2-substituted 3-aryl-4(3 Tetrahedron 62 9787-9826
12345678910