Synthesis of thiols from isobornylphenols

被引：0
作者：
I. Yu. Chukicheva
O. V. Sukrusheva
A. V. Kutchin
机构：
[1] Russian Academy of Sciences,Institute of Chemistry, Komi Scientific Center, Ural Branch
来源：
Russian Journal of Organic Chemistry | 2017年 / 53卷
关键词：
D O I：
暂无
中图分类号：
学科分类号：
摘要：
4-(3-Sulfanylpropyl)-2-isobornyl-6-methylphenol and 4-(sulfanylmethyl)-2,6-diisobornylphenol were synthesized from the corresponding 4-(bromoalkyl)phenols according to known procedures. Isobornylphenol with a trimethylene linker was converted into thiol by alkaline hydrolysis of thiouronium salt. The methylene-bridged analog was obtained by reduction of S-benzyl thioacetate with LiAlH4.
引用
收藏
页码：520 / 524
页数：4
相关论文
共 44 条
[1]  
Pinko P.I.(2002)undefined Russ. J. Appl. Chem. 75 1660-undefined
[2]  
Terakh E.I.(2008)undefined Russ. J. Bioorg. Chem. 34 499-undefined
[3]  
Gorokh E.A.(2007)undefined Biochemistry (Moscow) 72 644-undefined
[4]  
Nikulina V.V.(2011)undefined Chem. Sustainable Dev. 19 545-undefined
[5]  
Prosenko A.E.(2010)undefined Russ. Chem. Bull., Int. Ed. 59 2276-undefined
[6]  
Grigor’ev I.A.(2006)undefined Tetrahedron Lett. 47 8255-undefined
[7]  
Kemelev E.A.(2016)undefined Russ. J. Gen. Chem. 86 2052-undefined
[8]  
Vasyunina E.A.(2016)undefined Russ. Chem. Bull., Int. Ed. 65 1232-undefined
[9]  
Sinitsina O.I.(undefined)undefined undefined undefined undefined-undefined
[10]  
Khomchenko A.S.(undefined)undefined undefined undefined undefined-undefined
12345