Synthesis, characterization, and crystal structure of one zinc(II) complex with 4-Hydroxypyridine-2,6-Dicarboxylic acid and 4,4′-bipyridine

被引:0
作者
C. J. He
J. Q. Chen
机构
[1] Luoyang Normal University,Life Science Department
[2] Henan Industrial School,Student Management Office
来源
Russian Journal of Coordination Chemistry | 2014年 / 40卷
关键词
Coordination Chemistry; Coordination Polymer; Bipy; Pyridine Carboxyl; Bipy Ligand;
D O I
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中图分类号
学科分类号
摘要
A new zinc(II) coordination polymer, {[Zn(HCAM)(4,4′-Bipy)0.5] · H2O}n (I) (H3CAM = 4-hydroxypyridine-2,6-dicarboxylic acid; 4,4′-Bipy = 4,4′-bipyridine), has been synthesized by hydrothermal reaction of Zn(OAc)2, H3CAM and 4,4′-Bipy. It has been structurally characterized by element analysis, IR-spectra. X-ray single-crystal analysis was carried out for I (CIF file CCDC no. 974199), which crystallizes in the orthorhombic system, space group Pbca. The single X-ray diffraction studies reveal that I shows a new 2D wave-like plane with 3-connected net. Furthermore, the thermal stability of compound I was studied.
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页码:659 / 663
页数:4
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