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FT-IR, 1H NMR, 13C NMR and X-ray crystallographic structure determination of 4-nitro-benzenesulfonic acid 2,4-bis-(1-phenyl-ethyl)-naphthalen-1-yl ester
被引：0
|作者：
M. Kayalvizhi
G. Vasuki
A. Veerareddy
B. Sreenivasulureddy
A. Veerabhadrarao
机构：
[1] Kunthavai Naachiar Government Arts College (w) Autonomous,Department of Physics
[2] Suven Life Sciences Limited,R & D Laboratories
[3] Pondicherry University,Department of Chemistry
来源：
Journal of Structural Chemistry
|
2015年
/
56卷
关键词：
Title Compound;
Sulfonyl Chloride;
Benzenesulfonic Acid;
Benzene Sulfonyl Chloride;
Naphthalene Unit;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The title compound C32H27NO5S belongs to the monoclinic system, space group P21/c with a = 14.4530(5) Å, b = 13.9185(5) Å, c = 13.5714(4) Å, α = γ = 90°, β = 87.174(3)°, V = 2726.76(16) Å3, Z = 4, Dc = 1.310 g/cm3, F(000) = 1128, R = 0.053 and wR = 0.133, S = 1.03, T = 296 K. In the title compound, the naphthalene unit is planar (r.m.s. deviation = 0.0227 Å). The dihedral angle between the naphthalene unit and nitro-benzenesulfonic acid, 2-phenyl-ethyl and 4-phenyl-ethyl are 49.68(05)°, 82.96(06)°, and 81.94(07)° respectively. The structure is stabilized by intra- and intermolecular C-H…O hydrogen bonds.
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页码：392 / 395
页数：3
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