Synthesis of bis[2-methoxy-4-(11-oxo-7,8,9,10,11,12-hexahydrobenzo[a]acridin-12-yl)phenyl] succinates

被引：0

作者：

N. G. Kozlov

E. A. Dikusar

B. A. Odnoburtsev

机构：

[1] National Academy of Sciences of Belarus,Institute of Physical Organic Chemistry

来源：

Russian Journal of Organic Chemistry | 2008年 / 44卷

关键词：

Succinate; Schiff Base; Dimedone; Vanillal; HEXAHYDRO;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Reactions of succinyl chloride with 4-hydroxy-3-methoxybenzaldehyde and 3-ethoxy-4-hydroxybenzaldehyde gave the corresponding succinates which were brought into the condensation with naphthalen-2-amine to obtain Schiff bases. The latter reacted with CH acids (cyclohexane-1,3-dione and 5,5-dimethylcyclohexane-1,3-dione) to form bis[2-alkoxy-4-(11-oxo-7,8,9,10,11,12-hexahydrobenzo[a]acridin-12-yl)phenyl]-succinates which can also be obtained by three-component heterocyclization of naphthalen-2-amine with bis-(2-alkoxy-4-formylphenyl)succinates and CH acid.

引用

共 8 条

[1] Synthesis of bis[2-methoxy-4-(11-oxo-7,8,9,10,11,12-hexahydrobenzo[a]acridin-12-yl)phenyl] succinates
Kozlov, N. G.
Dikusar, E. A.
Odnoburtsev, B. A.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 44 (10) : 1504 - 1507
[2] Synthesis and spectral characteristics of 4-(10,10-dimethyl-8-oxo-7,8,9,10,11,12-hexahydrobenzo[c]acridin-7-yl)-2-methoxy(ethoxy)phenyl carboxylates
Skatetskii, V. V.
Kozlov, N. G.
Dikusar, E. A.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 43 (10) : 1481 - 1487
[3] Synthesis and spectral characteristics of 4-(10,10-dimethyl-8-oxo-7,8,9,10,11,12-hexahydrobenzo[c]acridin-7-yl)-2-methoxy(ethoxy)phenyl carboxylates
V. V. Skatetskii
N. G. Kozlov
E. A. Dikusar
Russian Journal of Organic Chemistry, 2007, 43 : 1481 - 1487
[4] Synthesis of methyl 12-aryl-9,9-dimethyl-11-oxo-7,8,9,10,11,12-hexahydrobenzo[a]acridine-10-carboxylate
N. G. Kozlov
S. L. Bondarev
A. P. Kadutskii
L. I. Basalaeva
Russian Journal of Organic Chemistry, 2010, 46 : 202 - 208
[5] Synthesis of methyl 12-aryl-9,9-dimethyl-11-oxo-7,8,9,10,11,12-hexahydrobenzo[a]acridine-10-carboxylate
Kozlov, N. G.
Bondarev, S. L.
Kadutskii, A. P.
Basalaeva, L. I.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (02) : 202 - 208
[6] Synthesis of 7-[4-alkoxy-3-methoxy(hydroxy)phenyl]-10,11-dihydrobenzo[c]acridin-8(7H,9H,12H)-ones and 4-(8-oxo-7,8,9,10,11,12-hexahydrobenzo[c]acridin-7-yl)-2-methoxy(ethoxy)phenyl esters of carboxylic acids
Kozlov, N. G.
Basalaeva, L. I.
Odnoburtsev, B. A.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (05) : 740 - 745
[7] Synthesis of 7-[4-alkoxy-3-methoxy(hydroxy)phenyl]-10,11-dihydrobenzo[c]acridin-8(7H,9H,12H)-ones and 4-(8-oxo-7,8,9,10,11,12-hexahydrobenzo[c]acridin-7-yl)-2-methoxy(ethoxy)phenyl esters of carboxylic acids
N. G. Kozlov
L. I. Basalaeva
B. A. Odnoburtsev
Russian Journal of Organic Chemistry, 2010, 46 : 740 - 745
[8] Synthesis of methyl 7-aryl(hetaryl, cyclohexenyl)-10-(1,3-benzodioxol-5-yl)-8-oxo-7,8,9,10,11,12-hexahydro-benzo[b][1,7]phenanthroline-9-carboxylates
N. G. Kozlov
A. B. Tereshko
Russian Journal of Organic Chemistry, 2013, 49 : 1335 - 1343

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