Bis[(18-crown-6)potassium] tetrakis(isothiocyanato)zinc(II): synthesis and crystal structure

被引：0

作者：

A. N. Chekhlov

机构：

[1] Russian Academy of Sciences,Institute of Problems of Chemical Physics

来源：

Russian Journal of Inorganic Chemistry | 2008年 / 53卷

关键词：

Complex Cation; Potassium Cation; Potassium Atom; Potassium Thiocyanate; Isothiocyanato;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A new complex, bis[(18-crown-6)potassium] tetrakis(isothiocyanato)zinc(II) [[K(18-crown-6)2] [Zn(NCS)4]] (I), is synthesized. Its crystal structure is studied using X-ray diffraction analysis (space group Pna21, a = 17.604 Å, b = 14.190 Å, c = 17.625 Å, Z = 4) by a direct method and refined by the full-matrix least-squares method in the anisotropic approximation to R = 0.099 for all 3994 measured independent reflections (CAD4 automated diffractiometer, λMoKα radiation).

引用

页码：780 / 784

页数：4

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