β-Cyclodextrin nanosponge polymer: a basic and eco-friendly heterogeneous catalyst for the one-pot four-component synthesis of pyranopyrazole derivatives under solvent-free conditions

被引:0
作者
Mina Jafari Nasab
Ali Reza Kiasat
Raziyeh Zarasvandi
机构
[1] Shahid Chamran University of Ahvaz,Department of Chemistry, College of Science
[2] Shahid Chamran University of Ahvaz,Petroleum Geology and Geochemistry Research Centre (PGGRC)
来源
Reaction Kinetics, Mechanisms and Catalysis | 2018年 / 124卷
关键词
β-Cyclodextrin-epichlorohydrin nanosponge polymer; Pyranopyrazole derivatives; Spiro[indoline-3,4′-pyrano[2,3-c]pyrazole; Multicomponent reactions;
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摘要
β-Cyclodextrin-epichlorohydrin nanosponge polymer, β-CD/EP, was prepared from the stepwise polymerization of β-cyclodextrin with epichlorohydrin under basic conditions and characterized by FT-IR spectroscopy, thermogravimetric analysis, scanning electron microscopy and Brunauer–Emmett–Teller. An efficient synthesis of spiro[indoline-3,4′-pyrano[2,3-c]pyrazole] and pyranopyrazole derivatives is described using β-CD/EP as a stationary micro-vessel and basic heterogeneous catalyst via a four component reaction under solvent-free conditions.
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页码:767 / 778
页数:11
相关论文
共 123 条
[11]  
Dorr RT(1999)undefined Biotechnol Prog 15 135-2266
[12]  
Blanchard J(2005)undefined J Am Chem Soc 127 657-358
[13]  
Zhou J(2011)undefined Chem Soc Rev 40 2254-195
[14]  
Ritter H(2001)undefined Jpn Patent 136 898-45
[15]  
Zhang X(2013)undefined Acta Pharm 63 335-5758
[16]  
Wang C(2012)undefined Beilstein J Org Chem 8 2091-295
[17]  
Chen Y(1989)undefined J Polym Sci C 27 191-3230
[18]  
Liu Y(1998)undefined Carbohyd Res 308 37-660
[19]  
Lezcano M(2002)undefined FEBS J 269 5753-994
[20]  
Al-Soufi W(2002)undefined Arch Pharm 335 289-2206