NMR Characterization of the Higher Molecular Weight Byproducts Formed During the Synthesis of [PCl2N]3

被引:0
作者
Amy J. Heston
Debasish Banerjee
Peter L. Rinaldi
Claire A. Tessier
机构
[1] University of Akron,Department of Chemistry
来源
Journal of Inorganic and Organometallic Polymers and Materials | 2007年 / 17卷
关键词
phosphazene; polyphosphazene; NMR; HMQC; DOSY;
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摘要
The by-product chlorophosphazenes obtained from the reaction of PCl5 and NH4Cl at ∼ 140°, have been characterized by 2D 31P–15N HMQC and DOSY NMR spectroscopy. These NMR spectra show that the byproducts are a very complex mixture.
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页码:477 / 481
页数:4
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