The growth and characterization of 2,4-dinitro phenyl hydrazone of benzophenone and mixed crystals

被引：0
|
作者：
G. Madhurambal
P. Ramasamy
P. AnbuSrinivasan
M. Suganthi
G. Vasudevan
S. C. Mojumdar
机构：
[1] Nagapattinam,ADM College for Women
[2] Chennai,Crystal Growth Center
[3] Mayiladuthurai,AVC College
[4] University of Toronto,Department of Chemical Engineering and Applied Chemistry
[5] University of New Brunswick,undefined
来源：
Journal of Thermal Analysis and Calorimetry | 2008年 / 94卷
关键词：
benzophenone; characterization; DTA; mixed crystal; SHG efficiency; solution growth; TG;
D O I：
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中图分类号：
学科分类号：
摘要：
Good quality benzophenone (BP) crystals were grown by solution technique using CHCl3 as solvent by adopting slow evaporation method at room temperature. The grown crystals were subjected to various characterization studies to analyze its purity and applications. The condensation product 2,4-dinitro phenyl hydrazone of benzophenone (DNPBP) was prepared by adopting standard procedure. Then mixed crystal of BP and DNPBP was also grown by solution growth. Both the condensation product and mixed crystals were characterized by UV, FTIR, 1H NMR spectra. Thermal (TG and DTA) studies have proved to be very useful techniques not only to study the thermal properties of BP, DNPBP and mixed crystal but also to study their purity. Second harmonic generation (SHG) efficiency of the grown crystals was determined.
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页码：45 / 51
页数：6
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