Synthesis, characterization, and crystal structure of 2-amino-5-oxo-4-phenyl-4,5-dihydropyrano[3,2-c]chromene-3-carbonitrile

被引：0

作者：

S. Sharma

G. Brahmachari

B. Banerjee

R. Kant

V. K. Gupta

机构：

[1] University of Jammu,X

[2] Visva-Bharati (a Central University),ray Crystallography Laboratory, Post

来源：

Crystallography Reports | 2015年 / 60卷

关键词：

Title Compound; Crystallography Report; Malononitrile; Multicomponent Reaction; Carbonitrile;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The title compound, 2-amino-5-oxo-4-phenyl-4,5-dihydropyrano[3,2-c]chromene-3-carbonitrile was synthesized in excellent yield by one-pot multicomponent reaction and its crystal structure is determined by X-ray structure analysis. The crystals are monoclinic, sp. gr. P21/c, a = 9.0750(6), b = 13.2729(8), c = 12.6892(9) Å, β = 96.975(6)°, Z = 4; R = 0.0466 for 1771 observed reflections. The crystal structure is stabilized by N–H···N, N–H···O and C–H···O hydrogen bonds. In addition, C–H···π and π···π interactions are observed in the crystal structure.

引用

页码：1142 / 1146

页数：4

共 50 条

[1] X-ray studies of 2-amino-5-oxo-4-propyl-4,5-dihydropyrano[3,2-c]chromene-3-carbonitrile
S. Sharma
B. Banerjee
G. Brahmachari
R. Kant
V. K. Gupta
Crystallography Reports, 2015, 60 : 865 - 868
[2] Synthesis, Characterization, and Crystal Structure of 2-Amino-7-methyl-5-oxo-4-phenyl-4,5-dihydropyrano[3,2-c]pyran-3-carbonitrile
Sharma, S.
Banerjee, B.
Brahmachari, G.
Kant, Rajni
Gupta, V. K.
CRYSTALLOGRAPHY REPORTS, 2015, 60 (07) : 1126 - 1130
[3] Synthesis, characterization, and crystal structure of 2-amino-7-methyl-5-oxo-4-phenyl-4,5-dihydropyrano[3,2-c]pyran-3-carbonitrile
S. Sharma
B. Banerjee
G. Brahmachari
Rajni Kant
V. K. Gupta
Crystallography Reports, 2015, 60 : 1126 - 1130
[4] A Simple Green Approach to the Synthesis of 2-Amino-5-oxo-4,5-dihydropyrano[3,2-c]chromene-3-carbonitrile Derivatives Catalyzed by 3-Hydroxypropanaminium Acetate (HPAA) as a New Ionic Liquid
Shaterian, H. R.
Oveisi, A. R.
JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2011, 8 (02) : 545 - 552
[5] A simple Green approach to the synthesis of 2-amino-5-oxo-4,5-dihydropyrano[3,2-c]chromene-3-carbonitrile derivatives catalyzed by 3-hydroxypropanaminium acetate (HPAA) as a new ionic liquid
H. R. Shaterian
A. R. Oveisi
Journal of the Iranian Chemical Society, 2011, 8 : 545 - 552
[6] X-ray studies of 2-amino-4-(3-nitrophenyl)-5-oxo-4,5-dihydropyrano[3,2-c] chromene-3-carbonitrile and 2-amino-7,7-dimethyl-4-(4-nitrophenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile
S. Sharma
B. Banerjee
G. Brahmachari
R. Kant
V. K. Gupta
Crystallography Reports, 2015, 60 : 1136 - 1141
[7] Crown ether complex cation ionic liquids (CECILs) as environmentally benign catalysts for three-component synthesis of 4,5-dihydropyrano[3,2-c]chromene and 4,5-dihydropyrano[4,3-b]pyran derivatives
Mehdi Abaszadeh
Mohammad Seifi
Research on Chemical Intermediates, 2015, 41 : 7715 - 7723
[8] Cross reactions of cyanoacetic acid derivatives with carbonyl compounds 3. One-step synthesis of substituted 2-amino-5-oxo-4,5-dihydropyrano[3,2-c]chromenes
A. A. Shestopalov
L. A. Rodinovskaya
A. M. Shestopalov
V. P. Litvinov
Russian Chemical Bulletin, 2005, 54 : 992 - 996
[9] Cross reactions of cyanoacetic acid derivatives with carbonyl compounds 3.: One-step synthesis of substituted 2-amino-5-oxo4,5-dihydropyrano[3,2-c]chromenes
Shestopalov, AA
Rodinovskaya, LA
Shestopalov, AM
Litvinov, VP
RUSSIAN CHEMICAL BULLETIN, 2005, 54 (04) : 992 - 996
[10] Crown ether complex cation ionic liquids (CECILs) as environmentally benign catalysts for three-component synthesis of 4,5-dihydropyrano[3,2-c]chromene and 4,5-dihydropyrano[4,3-b]pyran derivatives
Abaszadeh, Mehdi
Seifi, Mohammad
RESEARCH ON CHEMICAL INTERMEDIATES, 2015, 41 (10) : 7715 - 7723

← 1 2 3 4 5 →