Essential and Non-essential Work of Fracture of PI/SiO2 Hybrid Thin Films

被引:0
作者
Z. D. Wang
J. J. Lu
机构
[1] Beijing JiaoTong University,Institute of Engineering Mechanics
[2] Chinese Academy of Sciences,Institute of Mechanics
来源
Applied Composite Materials | 2007年 / 14卷
关键词
thin film; fracture; plane-stress condition; EWF; SEM; FE method;
D O I
暂无
中图分类号
学科分类号
摘要
Essential work of fracture (EWF) analysis is used to study the effect of the silica doping level on fracture toughness of polyimide/silica (PI/SiO2) hybrid films. By using double-edge-notched-tension (DENT) specimens with different ligament lengths, it seems that the introduction of silica additive can improve the specific essential work of fracture (we) of PI thin films, but the specific non-essential work of fracture (βwp) will decease significantly as the silica doping level increasing from 1 to 5 wt.%, and even lower than that of neat PI. The failure process of the fracture is investigated with online scanning electron microscope (SEM) observation and the parameters of non-essential work of fracture, β and wp, are calculated based on finite element (FE) method.
引用
收藏
页码:33 / 45
页数:12
相关论文
共 30 条
[1]  
Vlassak J.J.(1992)A new bulge testing technique for the determination of Young’s modulus and Possion’s ratio of thin films J. Mater. Res. 7 3242-3249
[2]  
Nix W.D.(1996)Determining mean and gradient residual stress in thin films using micromachined cantilevers J. Micromech. Microeng. 6 301-309
[3]  
Fang W.(1996)Thermal conductivity measurements on thin films based on micromechanical devices J. Micromech. Microeng. 6 118-121
[4]  
Wickert J.A.(2000)Synthesis and characterization of nanocomposite of polyimide-silica hybrid film nanoaqueous sol–gel process J. Appl. Phym. Sci. 76 1609-1618
[5]  
Jansen E.(2000)Mechanical properties of clay-polyimide (BTDA-ODA) nanocomposites via ODA-modified organnoclay J. Polyl. Sci. Part B: Polym. Phys. 38 2873-2878
[6]  
Obermeier E.(1968)Plane strain deformation near a crack tip in a power-law hardening materials J. Mech. Phys. Solids 16 1-12
[7]  
Hsiue G.H.(1975)On stable crack growth J. Mech. Phys. Solids 23 215-237
[8]  
Chen J.K.(2001)Fracture behaviour of polypropylene films at different temperatures: assessment of the EWF parameters Polymer 42 2665-2674
[9]  
Liu Y.L.(2002)Fracture of polybutylene temperature (PBT) film Polym. Test. 43 4033-4041
[10]  
Tyan H.L.(2003)Effect of temperature on fracture toughness of an amorphous poly(ether–ether ketone) film using essential work of fracture analysis Polym. Test. 22 589-599