Crystal structure of 1-acetyl-3-(4-methylphenyl)-5-phenyl-4,5-dihydro-1H-pyrazole

被引:0
|
作者
H. Bülbül
F. Tinmaz
N. Dege
İ. Özer İlhan
E. Sarıpınar
机构
[1] Ondokuz Mayıs University,Department of Physics, Faculty of Arts and Sciences
[2] Erciyes University,Department of Physics, Faculty of Sciences
来源
Crystallography Reports | 2014年 / 59卷
关键词
Pyrazole; Crystallography Report; Phenyl Hydrazine; Pyrazolines; Acetohydrazide;
D O I
暂无
中图分类号
学科分类号
摘要
In the title compound, C18H18N2O, the whole molecule is not planar but the phenyl ring systems are planar individually. The central pyrazole ring system is twisted with puckering parameters Q = 0.1610(18) Å and φ = 82.2(6)°. The crystallographic structure is stabilized by C-H⋯N type intramolecular hydrogen bond, generating ring motif R(5).
引用
收藏
页码:1071 / 1073
页数:2
相关论文
共 50 条
  • [31] 3-(4-Bromophenyl)-1-carbamothioyl-5-(2-carbamothioylhydrazinyl)-4,5-dihydro-1H-pyrazole-5-carboxylic Acid
    Andreeva, Anastasia A.
    Dmitriev, Maksim V.
    Maslivets, Andrey N.
    MOLBANK, 2024, 2024 (01)
  • [32] Crystal structure of 3-methyl-5-trimethylsilyl-1H-pyrazole
    Ferrence, Gregory M.
    Kocher, Joshua L.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O397 - U255
  • [33] Hypothermic and antipyretic effects of 3-methyl- and 3-phenyl-5-hydroxy5-trichloromethyl-4,5-dihydro-1H-pyrazole-l-carboxyamides in mice
    Souza, FR
    Souza, VT
    Ratzlaff, V
    Borges, LP
    Oliveira, MR
    Bonacorso, HG
    Zanatta, N
    Martins, MAP
    Mello, CF
    EUROPEAN JOURNAL OF PHARMACOLOGY, 2002, 451 (02) : 141 - 147
  • [34] SYNTHESIS, DIMERIC CRYSTAL STRUCTURE, AND FUNGICIDAL ACTIVITY OF 1-(4-METHYLPHENYL)-2-(5-((3,5-DIMETHYL-1H-PYRAZOL-1-YL)METHYL)-4-PHENYL-4H-1,2,4-TRIAZOL-3-YLTHIO)ETHANONE
    Liu, Xing-Hai
    Tan, Cheng-Xia
    Weng, Jian-Quan
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2011, 186 (03) : 558 - 564
  • [35] One-Pot Synthesis and Crystal Structure of Methyl 5-Hydroxy-1-phenyl-1H-pyrazole-3-carboxylate
    Saeed, Aamer
    Arshad, Ifzan
    Floerke, Ulrich
    CRYSTALS, 2012, 2 (03): : 1248 - 1252
  • [36] The molecular structure of 1,3-dimethyl-4-phenyl-1H-pyrazole-5-carboxylic acid
    Fernandez-Fernandez, Cristina
    Jagerovic, Nadine
    Alkorta, Ibon
    Maya, Celia M.
    Infantes, Lourdes
    Elguero, Jose
    ARKIVOC, 2008, : 74 - 84
  • [37] 4-Bromo-3-methoxy-1-phenyl-1H-pyrazole
    Kleiziene, Neringa
    Arbaciauskiene, Egle
    Holzer, Wolfgang
    Sackus, Algirdas
    MOLBANK, 2009, (04)
  • [38] Crystal structure of N′-(4-nitrobenzylidene)-5phenyl-1H-pyrazole-3-carbohydrazide, C17H13N5O3
    Karrouchi, Khalid
    Radi, Smaail
    Ansar, M'hammed
    Taoufik, Jamal
    Ghabbour, Hazem A.
    Mabkhot, Yahia N.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (03): : 839 - 841
  • [39] Simple and Efficient One-Pot Synthesis, Spectroscopic Characterization and Crystal Structure of Methyl 5-(4-Chlorobenzoyloxy)-1-phenyl-1H-pyrazole-3-carboxylate
    Khan, Imtiaz
    White, Jonathan M.
    CRYSTALS, 2012, 2 (03): : 967 - 973
  • [40] Microwave-assisted green synthesis of 4,5-dihydro-1H-pyrazole-1-carbothioamides in water
    Farmani, Hamid Reza
    Mosslemin, Mohammad Hossein
    Sadeghi, Bahareh
    MOLECULAR DIVERSITY, 2018, 22 (03) : 743 - 749